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Submicrosecond X-Ray Diffraction Studies*

Published online by Cambridge University Press:  06 March 2019

A. C. Mitchell
Affiliation:
Lawrence Livermore Laboratory, University of California, Livermore, California 94550
Quintin Johnson
Affiliation:
Lawrence Livermore Laboratory, University of California, Livermore, California 94550
L. Evans
Affiliation:
Lawrence Livermore Laboratory, University of California, Livermore, California 94550
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Abstract

As a result of interest stemming from shock wave studies carried out at Lawrence Livermore Laboratory, we have developed a capability to conduct x-ray diffraction studies in submicrosecond time intervals. This involves the use of a low impedance flash x-ray device. While there are many applications to which these techniques can be put, our first experiments deal with samples undergoing shock wave compression. These particular experiments are conducted by synchronizing a 40 to 50 nsec flash x-ray device to a shock front which is produced by the detonation of a high explosive placed in contact with a sample. Diffracted radiation is usually recorded on very sensitive film protected by a blast cassette. Thus far we have subjected lithium fluoride, aluminum, and carbon to pressures in the range of 100 to 300 kbar. Either powder or single crystal samples can be used. The principal difficulties of this experiment are the lack of sufficient intensity and the synchronization of the x-ray pulse to the shock front.

Type
Research Article
Copyright
Copyright © International Centre for Diffraction Data 1972

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Footnotes

*

Work performed under the auspices of the U. S. Atomic Energy Commission.

References

1. Charbonnier, F. M., “Proposed Flash X-Ray System for X-Ray Diffraction with Submicrosecond Exposure Time,” in Heinrich, K. F. J., Barrett, C. S., Newkirk, J. B., and Ruud, C. O., Editors, Advances in X'Ray Analysis, Vol. 15, p. 446 Plenum Press (1972).Google Scholar
2. Schall, R., “Microstructure Photography with Ultra-Short Exposures by Means of X-Ray Flash Tubes,Zeit, für Ang. Physik 11, 83 (1950).Google Scholar
3. Jamet, F., “Laue Diagrams by Instantaneous X-Ray Photography,C. R. Acad. Sci. Paris 271, 714 (1970).Google Scholar
4. Krehl, P.,“Generation of X-Ray Flash Interferences,” to be published.Google Scholar
5. Johnson, Q., Keeler, R. N. and Lyle, J. W., “X-Ray Diffraction Experiments in Nanosecond Time Intervals,Nature 213, 1114 (1967).Google Scholar
6. Johnson, Q., Mitchell, A. Keeler, R. N., and Evans, L., “Nanosecond X-Ray Diffraction: Study of Solids Under Shock Compression,” Trans. Amer. Crystallog. Assn. 4, 133,(1969).Google Scholar
7. Johnson, Q., Mitchell, A. Keeler, R. N., and Evans, L.,” X-Ray Diffraction During Shock-Wave Compression,” Phys. Rev. Lett. 25, 1099 (1970).Google Scholar
8. Johnson, Q., Mitchell, A. and Evans, L., “X-Ray Diffraction Evidence for Crystalline Order and Isotropie Compression during the Shock-Wave Process,Nature 231, 310 (1971).Google Scholar
9. Johnson, Q., Mitchell, A. and Evans, L., “X-Ray Diffraction Study of Single Crystals Undergoing Shock-Wave Compression,Appl. Phys. Lett. 21, 29 (1972).Google Scholar
10. Rice, M. H., McQueen, R. G., and Walsh, J. M., “Compression of Solids by Strong Shock Waves,” Solid State Physics. Vol. 6, p. 1, Academic Press (1958).Google Scholar
11. Duvall, G. E., “Some Properties and Applications of Shock Waves,” Air Force Office of Scientific Research, Washington, D. C. Rept. AFOSR TN 60-1185 (1960).Google Scholar
12. Al'tshuler, L. V., “Use of Shock Waves in High-Pressure Physics,Usp. Fiz. Nauk 85, 197 (1965).Google Scholar
13. Zeldovich, Ya. B. and Raizer, Yu. P., Physics of Shock Waves and High Temperature Hydrodynamic Phenomena, Vol 2, p. 685784 Acadtimic Press (1967).Google Scholar
14. Zharkov, V. N. and Kalinin, V. A., Equations of State for Solids at High Pressures and Temperatures, Consultants Bureau, New York (1971).Google Scholar
15. Blumlein, A. D., “Improvements in or Relating to Apparatus for Generating Electrical Impulses,” British Patent No. 589127, 12 June 1947.Google Scholar
16. Schaaffs, W., “X-Ray Flash Interferences,” German Patent No. 842974, 3 July 1952.Google Scholar
17. Ohlin, P and Händel, S., “Experiments with a Low Inductance High Vacuum X-Ray Flash Tube Set,Arkiv für Fysik 17, 157 (1960).Google Scholar
18. Zavada, N. I., Manokova, M. A., and Tsukerman, V. A., “Recording of Interferences of Monocrystals and Polycrystals with Microsecond Exposures,Prib. i Tekhn, Eksperim. No. 2, 434 (1966).Google Scholar
19. Jamet, F., “Recording of X-Ray Diffraction Patterns Using Flash X-Rays in Connection With an Image Intensifier,J. SMPTE 80, 900 (1971).Google Scholar
20. Martin, J. C., “Nanosecond Pulse Techniques,” United Kingdom Atomic Energy Association, Berkshire, Rept, SSWA/JCM/704/49 (1970).Google Scholar
21. Johnson, Q., Mitchell, A. and Evans, L., “X-Ray Detector for Dynamic Diffraction Studies,Rev. Sci. Inst. 42, 999 (1971).Google Scholar
22. Swan, William, private communication, 1971.Google Scholar
23. Mitchell, A., Johnson, Q. and Evans, L., “Film Cassette for Flash X-Ray Studies of Shock Wave Events,” to be published.Google Scholar
24. Seemann, H., “A Focusing X-Ray Spectroscopic Arrangement for Powders,Ann. Physik 59, 455 (1919).Google Scholar
25. Bohlin, H., “A New Arrangement for X-Ray Crystallographic Investigations of Powders,Ann. Physik, 61, 421 (1920).Google Scholar
26. Christian, R. A., “The Equation of State of the Alkali Halides at High Pressure,” Lawrence Radiation Laboratory, Livermore, Rept. 4900 (1957).Google Scholar
27. Al'tshuler, L. V., Brazknik, M. I., German, V. N., and Mirkin, L. I., “Explosive Deformation of Single Crystals,Sov. Phys. Solid State 9, 2417 (1968).Google Scholar
28. Hauver, G. E. and Melani, A., “The Shock Hugoniot of Single-Crystal Lithium Fluoride,” Ballistic Research Laboratories, Aberdeen Proving Ground, Rept. 2058 (1970).Google Scholar
29. van Thiel, M., Kusubov, A. S., and Mitchell, A. C., “Shock Wave Data,” Lawrence Livermore Laboratory, Rept. UCRL-50108 (1966).Google Scholar
30. Lynch, R. W. and Drickamer, H. G., “Effect of High Pressure on the Lattice Parameters of Diamond, Graphite, and Hexagonal Boron Nitride,J. Chem. Phys. 44, 181 (1966).Google Scholar
31. Coleburn, N. L., “Compressibility of Pyrolytic Graphite,Phys J. Chem., 40, 71 (1964).Google Scholar