Hostname: page-component-78c5997874-v9fdk Total loading time: 0 Render date: 2024-11-19T10:51:21.350Z Has data issue: false hasContentIssue false

Additive controlled crystallization of barium titanate powders and their application for thin-film ceramic production: Part I. Powder Synthesis

Published online by Cambridge University Press:  31 January 2011

B. Grohe
Affiliation:
Max Planck-Institut für Polymerforschung, Ackermannweg 10, D-55128 Mainz, FRG
G. Miehe
Affiliation:
Technische Universität Darmstadt, Fachbereich Materialwissenschaft, Petersenstraβe 23, D-64287 Darmstadt, FRG
G. Wegner*
Affiliation:
Max Planck-Institut für Polymerforschung, Ackermannweg 10, D-55128 Mainz, FRG
*
a)Address all correspondence to this author.
Get access

Abstract

Stoichiometric barium titanate (BaTiO3) was synthesized in aqueous solution with acetone and/or methanol as additives to control the crystallization process. Adjusted nano-sized particles and narrow particle size distributions were achieved at 60 °C with additive concentrations up to 243 ml/ l. The growth kinetics showed that the additives influence the nucleation of the BaTiO3 particles and tend to suppress Ostwald ripening.

Type
Articles
Copyright
Copyright © Materials Research Society 2001

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1.Klee, M., J. Mater. Sci. Lett. 8, 985 (1989).CrossRefGoogle Scholar
2.Hagemann, H.J., Hennings, D., and Wernicke, R., Philips Tech. Rev. 41, 89 (1983/1984).Google Scholar
3.Phule, P.P. and Risbud, S.H., J. Mater. Sci. 25, 1169 (1990).Google Scholar
4.Hellebrand, H., in Material Science and Technology, Vol. 17A: Tape Casting, 1st ed., edited by Cahn, R.W., Haasen, P., and Kramer, E.J. (VCH Verlag, Weinheim, Germany, 1995), pp. 194195.Google Scholar
5.Her, Y-S. and Matijević, E., J. Mater. Res. 12, 3106 (1995).CrossRefGoogle Scholar
6.Chaput, F. and Boilot, J-P., Silic. Ind., Ceram. Sci. Technol. 11–12, 317 (1990).Google Scholar
7.Stockenhuber, M., Mayer, H., and Lercher, J.A., J. Am. Ceram. Soc. 76, 1185 (1993).Google Scholar
8.Pechini, M.P., U.S. Patent No. 3 330 697 (July 11, 1967).Google Scholar
9.Salez, H., Odier, P., and Cales, B., J. Non-Cryst. Solids 82, 314 (1986).CrossRefGoogle Scholar
10.Salez, H., Cales, B., and Odier, P., Mater. Sci. Monogr. (High Tech. Ceram.) 38A, 491 (1987).Google Scholar
11.Hennings, D. and Mayr, W., J. Solid State Chem. 26, 329 (1978).Google Scholar
12.Ali, N.J. and Milne, S.J., Trans. J. Br. Ceram. Soc. 86, 113 (1987).Google Scholar
13.Christensen, A.N., Acta Chem. Scand. 24, 2447 (1970).CrossRefGoogle Scholar
14.Kaneko, S. and Imoto, F., Nippon Kagaku Kaishi 6, 985 (1975).CrossRefGoogle Scholar
15.Kutty, T.R.N. and Balachandran, R., Mater. Res. Bull. 19, 1479 (1984).CrossRefGoogle Scholar
16.Murugaraj, P. and Kutty, T.R.N., Mater. Res. Bull. 20, 1473 (1985).CrossRefGoogle Scholar
17.Vivekanadan, R., Philip, S., and Kutty, T.R.N., Mater. Res. Bull. 22, 99 (1986).CrossRefGoogle Scholar
18.Maurice, A.K. and Buchanan, R.C., Ferroelectrics 74, 61 (1987).Google Scholar
19.Mazdiyasni, K.S., Dolloff, R.T., and Smith, J.S. II, J. Am. Ceram. Soc. 52, 523 (1969).CrossRefGoogle Scholar
20.Blendale, P., Venigalla, S., Ambrose, J.R., Verink, E.D. Jr., and Adair, J.H., J. Am. Ceram. Soc. 76, 2619 (1993).CrossRefGoogle Scholar
21.Kiss, K., Magder, J., Vukasovich, M.S., and Lockhart, R.J., J. Am. Ceram. Soc. 49, 291 (1966).CrossRefGoogle Scholar
22.Flaschen, S.S., J. Am. Ceram. Soc. 77, 6194 (1955).Google Scholar
23.Chaput, F. and Boilot, J.P., J. Mater. Sci. Lett. 6, 1110 (1987).Google Scholar
24.Wiles, D.B. and Young, R.A., J. Appl. Crystallogr. 14, 149 (1981).CrossRefGoogle Scholar
25.Howard, C.J. and Hill, R.J., Aust. A.E.C. Res. Establ. Rep. AAEC M112 (1986).Google Scholar
26.Kurzydlowski, K.J. and Ralph, B., The Quantitative Description of the Microstructure of Materials, 1st ed. (CRC Press, Boca Raton, New York, London, Tokyo, 1995), pp. 3747.Google Scholar
27.Keppel, G., Design and Analysis, 3rd ed. (Prentice Hall, Upper Saddle River, NJ, 1991), pp. 1108.Google Scholar
28.Sahner, H., Schließende Statistik, Statistik für Soziologen, 2nd ed., edited by Scheuch, E.K. (B.G. Teubner Verlag, Stuttgart, Germany, 1971), pp. 57174.Google Scholar
29.Arima, M., Kakihama, M., Nakamura, Y., Yashima, M., and Yashimura, M., J. Am. Ceram. Soc. 79, 2847 (1996).Google Scholar
30.Diaz-Guemes, M.I., Carreno, T.G., and Serna, C.J., J. Mater. Sci. 24, 1011 (1989).Google Scholar
31.Padmini, P. and Kutty, T.R.N., J. Mater. Chem. 4, 1875 (1994).Google Scholar
32.Lencka, M.M. and Riman, R.E., Chem. Mater. 5, 61 (1993).CrossRefGoogle Scholar
33.Slamovich, E.B. and Aksay, I.A., J. Am. Ceram. Soc. 79, 239 (1996).CrossRefGoogle Scholar
34.Atkins, P.W., Physical Chemistry, 3rd ed. (Oxford University Press, Oxford, U.K., 1986), pp. 654660.Google Scholar
35.Zhao, L., Chien, A.T., Lange, F.F., and Speck, J.S., J. Mater. Res. 11, 1325 (1996).CrossRefGoogle Scholar
36.Takeuchi, T., Tabuchi, M., Ado, K., Honjo, K., and Nakamura, O., J. Mater. Sci. 32, 4053 (1997).CrossRefGoogle Scholar
37.Sanchez, C., Livage, J., Henry, M., and Babonneau, F., J. Non-Cryst. Solids 100, 65 (1988).Google Scholar
38.Okuyama, M., Fukui, T., and Sakurai, C., J. Non-Cryst. Solids 143, 112 (1992).Google Scholar
39.Harris, M.T. and Byers, C.H., J. Non-Cryst. Solids 103, 49 (1988).CrossRefGoogle Scholar
40.Chen, K.C., Tsuchiya, T., and Mackenzie, J.D., J. Non-Cryst. Solids 81, 227 (1986).Google Scholar
41.Öye, G., Libnau, F.O., Sjöblom, J., and Friberg, S.E., Colloids Surf., A 123–124, 329 (1997).Google Scholar
42.Fukui, T., Sakurai, C., and Okuyama, M., J. Mater. Sci. 32, 189 (1997).Google Scholar
43.Nabavi, M., Doeuff, S., Sanchez, C., and Livage, J., J. Non-Cryst. Solids 121, 31 (1990).Google Scholar
44.Kleber, W., Bautsch, H-J., and Bohm, J., Einführung in die Kristal-lographie, 17th ed. (VEB Verlag Technik, Berlin, Germany, 1990), pp. 201206.Google Scholar
45.Raghavan, V. and Cohen, M., in Treatise on Solid State Chemistry: Solid-State Phase Transformations, edited by Hannay, N.B. (Plenum Press, New York, London, 1975), Vol. 5, p. 67.Google Scholar
46.Cölfen, H., Pauck, T., and Antonietti, M., Prog. Colloid Polym. Sci. 107, 136 (1997).CrossRefGoogle Scholar