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Determining the mechanical properties of small volumes of material from submicrometer spherical indentations

Published online by Cambridge University Press:  03 March 2011

J.S. Field  and
M.V. Swain
J.S. Field
Affiliation:
Department of Mechanical Engineering, University of Sydney, New South Wales, 2006, Australia, and CSIRO Division of Applied Physics, Lindfield, New South Wales, 2070, Australia
M.V. Swain
Affiliation:
Department of Mechanical Engineering, University of Sydney, New South Wales, 2006, Australia, and CSIRO Division of Applied Physics, Lindfield, New South Wales, 2070, Australia
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Abstract

The stress/strain behavior of bulk material is usually investigated in uniaxial tension or compression; however, these methods are not generally available for very small volumes of material. Submicrometer indentation using a spherical indenter has the potential for filling this gap with, possibly, access to hardness and elastic modulus profiles, representative stress/strain curves, and the strain hardening index. The proposed techniques are based on principles well established in hardness testing using spherical indenters, but not previously applied to depth-sensing instruments capable of measurements on a submicrometer scale. These approaches are now adapted to the analysis of data obtained by stepwise indentation with partial unloading, a technique that facilitates separation of the elastic and plastic components of indentation at each step and is able to take account of the usually ignored phenomena of “piling up” and “sinking in”.

Type
Articles
Information
Journal of Materials Research , Volume 10 , Issue 1 , January 1995 , pp. 101 - 112
Copyright
Copyright © Materials Research Society 1995

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References

REFERENCES

1Brinell, J. A., Congress Int. des Methods d'Essai des Mat. de Construction, Paris 2, 83 (1901).Google Scholar
2Field, J. S. and Swain, M. V., J. Mater. Res. 8, 297 (1993).CrossRefGoogle Scholar
3Francis, H. A., Trans. ASME (Series H) 9, 272 (1976).Google Scholar
4Hertz, H., J. reine u. angew. Math (Crelle) 92, 156 (1882).CrossRefGoogle Scholar
5Johnson, K. L., Contact Mechanics (Cambridge University Press, Cambridge, UK, 1985).CrossRefGoogle Scholar
6Tabor, D., Hardness of Solids (Oxford University Press, Oxford, UK, 1951).Google Scholar
7Meyer, E., Z. Ver Deutsch Ing. 52, 645 (1908).Google Scholar
8O'Neill, H., Proc. Inst. Mech. Eng. 151, 116 (1944).CrossRefGoogle Scholar
9Norbury, A. L. and Samuel, T., J. Iron Steel Inst. 117, 673 (1928).Google Scholar
10Rhee, S. S. and McClintock, F. M., Proc. 4th U.S. Natl. Cong. Appl. Mech., 1007 (1962).Google Scholar
11Mathews, J. R., Acta Metall. 28, 311 (1980).CrossRefGoogle Scholar
12Richmond, O., Morrison, H. L., and Devenpeck, M. L., Int. J. Mech. Sci. 16, 75 (1974).CrossRefGoogle Scholar
13Hill, R., Storåkers, B., and Zdunek, A.B., Proc. R. Soc. London A423, 301 (1989).Google Scholar
14Hill, R., J. Mech. Phys. Solids 35, 565 (1987).CrossRefGoogle Scholar
15Stillwell, N. A. and Tabor, D., Phys. Soc. Proc. 78, 169 (1961).CrossRefGoogle Scholar
16Oliver, W. C. and Pharr, G. M., J. Mater. Res. 7, 1564 (1992).CrossRefGoogle Scholar
17Loubet, J. L., Georges, J. M., and Meille, G., in Microindentation Techniques in Materials Science and Engineering, edited by Blau, P. J. and Lawn, B. R. (ASTM Special Technical Publication, Philadelphia, 1985), p. 72.CrossRefGoogle Scholar
18Doerner, M. F. and Nix, W. D., J. Mater. Res. 1, 601 (1986).CrossRefGoogle Scholar
19Sneddon, I. N., Int. J. Eng. Sci. 3, 47 (1965).CrossRefGoogle Scholar
20Doerner, M. F., Gardner, D. S., and Nix, W. D., J. Mater. Res. 1, 845 (1986).CrossRefGoogle Scholar
21Pharr, G. M. and Oliver, W. C., MRS Bull. (July 1992).Google Scholar
22Pharr, G. M., Oliver, W. C., and Brotzen, F. R., J. Mater. Res. 7, 613 (1992).CrossRefGoogle Scholar
23The Properties ofDiamond, edited by Field, J. E. (Academic Press, London, 1979).Google Scholar