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In situ x-ray observation of bainitic transformation of austempered silicon alloyed steel

Published online by Cambridge University Press:  31 January 2011

Xiang Chen*
Affiliation:
Division of Engineering Materials, Department of Applied Physics and Mechanical Engineering, Luleå University of Technology, SE-97187 Luleå, Sweden; and Key Laboratory for Advanced Materials Processing Technology, Ministry of Education of China, Department of Mechanical Engineering, Tsinghua University, 100084 Beijing, China
Esa Vuorinen
Affiliation:
Division of Engineering Materials, Department of Applied Physics and Mechanical Engineering, Luleå University of Technology, SE-97187 Luleå, Sweden
*
a) Address all correspondence to this author. \e-mail: xchen@mail.tsinghua.edu.cn
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Abstract

The in situ x-ray diffraction observations of the bainitic transformation were conducted by using the high-temperature x-ray diffraction technique. The volume fraction and carbon content of austenite depend on the transformation temperature. The d{110} value of bainitic ferrite decreases with increasing austempering temperature, which is related to the decrease of carbon concentration in bainitic ferrite. Asymmetry diffraction peaks are obtained for samples at the early stage of transformation at any austempering temperatures. This asymmetry diffraction peak after the formation of bainitic ferrite could be attributed to a heterogeneous distribution of carbon in different regions of austenite and show that two types of austenite with different carbon contents, low-carbon austenite (γLC) and the high-carbon austenite (γHC), exist during the transformation. The microstructure after cooling down to room temperature is presented to show the effectiveness of the x-ray diffraction analysis.

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Articles
Copyright
Copyright © Materials Research Society 2009

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References

1Bhadeshia, H.K.D.H. and Edmonds, D.V.: Analysis of mechanical properties and microstructure of high silicon dual phase steel. Meat Sci. 14, 41 (1980).CrossRefGoogle Scholar
2Voigt, R.C., Bendaly, R., Janowak, J.F., and Park, Y.L.: Development of austempered high silicon cast steel. AFS Transact. 93, 453 (1985).Google Scholar
3Park, Y.L., Gundlach, R.B., and Janowak, J.F.: Monitoring the bainite reaction during austempering of ductile iron and high silicon cast steel by resistively measurement. AFS Transact. 95, 411 (1987).Google Scholar
4Putatunda, S.K.: Fracture toughness of a high carbon and high silicon steel. Mater. Sci. Eng., A 297, 31 (2001).CrossRefGoogle Scholar
5Putatunda, S.K.: Influence of austempering temperature on micro-structure and fracture toughness of a high-carbon, high-silicon and high-manganese cast steel. Mater. Des. 24, 435 (2003).CrossRefGoogle Scholar
6Putatunda, S.K.: Austempering of a silicon manganese cast steel. Mater. Manuf. Processes 16, 743 (2001).CrossRefGoogle Scholar
7Li, Y.X. and Chen, X.: Microstructure and mechanical properties of austempered high silicon cast steel. Mater. Sci. Eng., A 308, 277 (2001).CrossRefGoogle Scholar
8Navara, E. and Zimba, J.: Ausferritic ferrous alloys—A challenge to industry and research. Acta Metall. Slovaca. 10, 244 (2004).Google Scholar
9Chen, X. and Li, Y.X.: Fracture toughness improvement of austempered high silicon steel by titanium, vanadium and rare earth elements multi-element modification. Mater. Sci. Eng., A 444, 298 (2007).CrossRefGoogle Scholar
10Lee, Y.K., Shin, H.C., Jang, Y.C., and Kim, S.H.: Effect of isothermal transformation temperature on amount of retained austenite and its thermal stability in a bainitic Fe-3%Si-0.45%C-X steel. Scr. Mater. 47, 805 (2002).CrossRefGoogle Scholar
11Liu, C., Zhao, Z., and Bhole, S.D.: Lathlike upper bainite in a silicon steel. Mater. Sci. Eng., A 434, 289 (2006).CrossRefGoogle Scholar
12Miihkinen, V.T.T. and Edmonds, D.V.: Microstructural examination of two experimental high-strength bainitic low-alloy steels containing silicon. Mater. Sci. Technol. 3, 422 (1987).CrossRefGoogle Scholar
13Miihkinen, V.T.T. and Edmonds, D.V.: Tensile deformation of two-experimental high-strength bainitic low-alloy steels containing silicon. Mater. Sci. Technol. 3, 432 (1987).CrossRefGoogle Scholar
14Miihkinen, V.T.T. and Edmonds, D.V.: Fracture toughness of two experimental high-strength bainitic low-alloy steels containing silicon. Mater. Sci. Technol. 3, 441 (1987).CrossRefGoogle Scholar
15Bhadeshia, H.K.D.H. and Edmonds, D.V.: Bainite in silicon steels: New composition-property approach. Part 1. Meat Sci. 17, 411 (1983).CrossRefGoogle Scholar
16Bhadeshia, H.K.D.H. and Edmonds, D.V.: Bainite in silicon steels: New composition-property approach. Part 2. Meat Sci. 17, 420 (1983).CrossRefGoogle Scholar
17Edmonds, D.V. and Cochrane, R.C.: Structure-property relationships in bainitic steels. Metall. Trans. A 21, 1527 (1990).CrossRefGoogle Scholar
18Babu, S.S., Specht, E.D., David, S.A., Karapetrova, E., Zschack, P., Peet, M., and Bhadeshia, H.K.D.H.: In-situ observations of lattice parameter fluctuations in austenite and transformation to bainite. Metall. Mater. Trans. A 36, 3281 (2005).CrossRefGoogle Scholar
19Stone, H.J., Peet, M.J., Bhadeshia, H.K.D.H., Withers, P.J., Babu, S.S., and Specht, E.D.: Synchrotron x-ray studies of austenite and bainitic ferrite. Proc. R. Soc. London, Sect. A 464, 1009 (2008).Google Scholar
20Caballero, F.G., Bhadeshia, H.K.D.H., Mawella, K.J.A., Jones, D.G., and Brown, P.: Design of novel high strength bainitic steels: Part 2. Mater. Sci. Technol. 17, 517 (2001).CrossRefGoogle Scholar
21Wang, Y-H.: Fundamental of X-Ray Diffraction Technology (Atomic Energy Press, Beijing, China, 1986), p. 159.Google Scholar
22Dyson, D.J. and Holmes, B.: Effect of alloying additions on the lattice parameter of austenite. ISIJ Int. 208, 469 (1970).Google Scholar