Hostname: page-component-788cddb947-nxk7g Total loading time: 0 Render date: 2024-10-19T00:06:35.271Z Has data issue: false hasContentIssue false
  • English
  • Français

Modified resin–intermediate processing of perovskite powders: Part II. Processing for fine, nonagglomerated Sr-doped lanthanum chromite powders

Published online by Cambridge University Press:  31 January 2011

Lone-Wen Tai  and
Paul A. Lessing
Lone-Wen Tai
Affiliation:
Ceramic Engineering Department, University of Missouri–Rolla, Rolla, Missouri 65401
Paul A. Lessing
Affiliation:
Ceramics Section, EG&G Idaho, Inc., Idaho National Engineering Laboratory, Idaho Falls, Idaho 83415
Get access

Abstract

Nonagglomerated ceramic precursor for Sr-doped lanthanum chromite powder was prepared by a modified resin–intermediate process using equimolar citric acid, ethylene glycol, and metallic nitrates. Pure and well-crystallized submicron powders with a narrow particle-size distribution were calcined from an optimally pulverized resin at a temperature of 750 °C for 2 h in flowing air. The material cost for organics used in the investigated process was considerably lower than the original Pechini process.

Type
Articles
Information
Journal of Materials Research , Volume 7 , Issue 2 , February 1992 , pp. 511 - 519
Copyright
Copyright © Materials Research Society 1992

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1.Eror, N. G. and Anderson, H. U., in Better Ceramics Through Chemistry II, edited by Brinker, C. J., Clark, D. E., and Ulrich, D. R. (Mater. Res. Soc. Symp. Proc. 73, Pittsburgh, PA, 1986), pp. 571–577.Google Scholar
2.Pechini, M. P., Pat, U. S.. No. 3 330697, July 11, (1967).Google Scholar
3. Paul Lessing, A., Am. Ceram. Soc. Bull. 68 (5), 1002–1007 (1989).Google Scholar
4.Tai, L. W. and Lessing, Paul A., J. Mater. Res. 7, 502–510 (1992).CrossRefGoogle Scholar
5.Lessing, P. A., Tai, L. W., and Klemm, K. A., in Proc. 1st Int. Symp. on Solid Oxide Fuel Cells, edited by Subhash Singhal, C. (Electrochemical Society, Pennington, NJ, 1989), pp. 337–360.Google Scholar
6.Carter, J. D. and Anderson, H. U., unpublished work.Google Scholar
7.Tai, L. W. and Lessing, P. A., J. Am. Ceram. Soc. 74 (1), 155–160 (1991).CrossRefGoogle Scholar