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Off-Axis Electron Holography of Unbiased and Reverse-Biased Focused Ion Beam Milled Si p-n Junctions

Published online by Cambridge University Press:  28 January 2005

Alison C. Twitchett
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge CB2 3QZ, UK
Rafal E. Dunin-Borkowski
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge CB2 3QZ, UK
Robert J. Hallifax
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge CB2 3QZ, UK
Ronald F. Broom
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge CB2 3QZ, UK
Paul A. Midgley
Affiliation:
Department of Materials Science and Metallurgy, University of Cambridge, Pembroke Street, Cambridge CB2 3QZ, UK
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Abstract

Off-axis electron holography is used to measure electrostatic potential profiles across a silicon p-n junction, which has been prepared for examination in the transmission electron microscope (TEM) in two different specimen geometries using focused ion beam (FIB) milling. Results are obtained both from a conventional unbiased FIB-milled sample and using a novel sample geometry that allows a reverse bias to be applied to an FIB-milled sample in situ in the TEM. Computer simulations are fitted to the results to assess the effect of TEM specimen preparation on the charge density and the electrostatic potential in the thin sample.

Type
MATERIALS APPLICATIONS
Copyright
© 2005 Microscopy Society of America

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References

REFERENCES

Beleggia, M., Cristofori, D., Merli, P.G., & Pozzi, G. (2000). Electron microscopy of reverse biased p-n junctions. Micron 31, 231236.Google Scholar
Beleggia, M., Fazzini, P.F., Merli, P.G., & Pozzi, G. (2003). Influence of charged oxide layers on TEM imaging of reverse-biased p-n junctions. Phys Rev B 67, 045328.Google Scholar
Darlington, E.H. & Valdré, U. (1975). Imaging of weak Lorentz objects (p-n junctions) by high voltage Fresnel TEM and STEM. J Phys E 8, 321324.Google Scholar
de Ruijter, W.J. & Weiss, J.K. (1993). Detection limits in quantitative off-axis electron holography. Ultramicroscopy 50, 269283.Google Scholar
Donnet, D.M., De Veirman, A.E.M., Otterloo, B., & Roberts, H. (2003). Novel FIB-TEM preparation methods for semiconductor device characterisation and failure analysis. Inst Phys Conf Ser 180, 617620.Google Scholar
Dunin-Borkowski, R.E., McCartney, M.R., & Smith, D.J. (2004). Electron holography of nanostructured materials. In Encyclopaedia of Nanoscience and Nanotechnology, Nalwa, H.S. (Ed.), Vol. 3, pp. 41100. Stevenson Ranch, California: American Scientific Publishers.
Frabboni, S., Matteucci, G., Pozzi, G., & Vanzi, M. (1985). Electron holographic observations of the electrostatic-field associated with thin reverse-biased p-n junctions. Phys Rev Lett 55, 21962199.Google Scholar
Houben, L., Luysberg, M., & Brammer, T. (2003). Electron beam illumination effects on electrostatic potential mapping in holographic imaging of semiconductors in transmission electron microscopy. Inst Phys Conf Ser 180, 4952.Google Scholar
Langford, R.M. & Petford-Long, A.K. (2001). Preparation of transmission electron microscopy cross-section specimens using focused ion beam milling. J Vac Sci Technol A 19, 21862193.Google Scholar
McCartney, M.R. & Gajdardziska-Josifovska, M. (1994). Absolute measurement of normalized thickness, t/λi, from off-axis electron holography. Ultramicroscopy 53, 283289.Google Scholar
McCartney, M.R., Gribelyuk, M.A., Li, J., Ronsheim, P., McMurray, J.S., & Smith, D.J. (2002). Quantitative analysis of one-dimensional dopant profile by electron holography. Appl Phys Lett 80, 32133215.Google Scholar
Merli, P.G., Missiroli, G.F., & Pozzi, G. (1974). P-n junction observations by interference electron microscopy. J de Microscopie 21, 1120.Google Scholar
Merli, P.G., Missiroli, G.F., & Pozzi, G. (1975). Electron microscopy observations of p-n junctions. Phys Stat Sol (a) 30, 699711.Google Scholar
Press, W.H., Flannery, B.P., Teukolsky, S.A., & Vetterling, W.T. (1989). Numerical Recipes. Cambridge, UK: Cambridge University Press.
Rau, W.D., Schwander, P., Baumann, F.H., Hoppner, W., & Ourmazd, A. (1999). Two-dimensional mapping of the electrostatic potential in transistors by electron holography. Phys Rev Lett 82, 26142617.Google Scholar
Saxton, W.O., Pitt, T.J., & Horner, M. (1979). Digital image processing: The Semper system. Ultramicroscopy 4, 343354.Google Scholar
Somodi, P.K., Dunin-Borkowski, R.E., Twitchett, A.C., Barnes, C.H.W., & Midgley, P.A. (2003). Simulations of the electrostatic potential distribution in a TEM sample of a semiconductor device. Inst Phys Conf Ser 180, 501504.Google Scholar
Sze, S.M. (2002). Semiconductor Devices. New York: Wiley.
Titchmarsh, J.M., Lapworth, A.J., & Booker, G.R. (1969). A new method for investigating the electric field regions of p-n junctions. Phys Stat Sol 34, K83K86.Google Scholar
Twitchett, A.C., Dunin-Borkowski, R.E., & Midgley, P.A. (2002). Quantitative electron holography of biased semiconductor devices. Phys Rev Lett 88, 238302.Google Scholar
Vanzi, M. (1984). Theoretical model for studying electrostatic potentials by means of Lorentz microscopy. Optik 68, 319333.Google Scholar
Wang, Z., Hirayama, T., Sasaki, K., Saka, H., & Kato, N. (2002a). Electron holographic characterization of electrostatic potential distributions in a transistor sample fabricated by focused ion beam. Appl Phys Lett 80, 246248.Google Scholar
Wang, Z., Kato, T., Shibata, N., Hirayama, T., Kato, N., Sasaki, K., & Saka, H. (2002b). Characterizing an implanted Si/Si p-n junction with lower doping level by combined electron holography and focused-ion-beam milling. Appl Phys Lett 81, 478480.Google Scholar
Williams, D.B. & Carter, C.B. (1997). Transmission Electron Microscopy. New York: Plenum Press.