Hostname: page-component-586b7cd67f-2brh9 Total loading time: 0 Render date: 2024-11-26T23:43:29.505Z Has data issue: false hasContentIssue false

Characterizing Multivalent Metal Anodes with Cryogenic Electron Microscopy

Published online by Cambridge University Press:  30 July 2021

Daniel Long
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico, United States
Scott McClary
Affiliation:
Sandia National Laboratories, United States
Paul Kotula
Affiliation:
Sandia National Laboratories, Albuquerque, New Mexico, United States
Kevin Zavadil
Affiliation:
Sandia National Laboratories, United States
Katherine Jungjohann
Affiliation:
Sandia National Laboratories, United States

Abstract

Image of the first page of this content. For PDF version, please use the ‘Save PDF’ preceeding this image.'
Type
Advanced Imaging and Spectroscopy for Nanoscale Materials Characterization
Copyright
Copyright © The Author(s), 2021. Published by Cambridge University Press on behalf of the Microscopy Society of America

References

Harrison, K. L.; Zavadil, K. R.; Hahn, N. T.; Meng, X.; Elam, J. W.; Leenheer, A.; Zhang, J. G.; Jungjohann, K. L., Lithium Self-Discharge and Its Prevention: Direct Visualization through in Situ Electrochemical Scanning Transmission Electron Microscopy. ACS Nano 2017, 11, 11194-11205.Google ScholarPubMed
Ponrouch, A.; Bitenc, J.; Dominko, R.; Lindahl, N.; Johansson, P.; Palacin, M. R., Multivalent Rechargeable Batteries. Energy Storage Materials 2019, 20, 253-262.Google Scholar
Zachman, M. J.; Asenath-Smith, E.; Estroff, L. A.; Kourkoutis, L. F., Site-Specific Preparation of Intact Solid-Liquid Interfaces by Label-Free in Situ Localization and Cryo-Focused Ion Beam Lift-Out. Microsc Microanal 2016, 22, 1338-1349.CrossRefGoogle ScholarPubMed
Rubino, S.; Akhtar, S.; Melin, P.; Searle, A.; Spellward, P.; Leifer, K., A Site-Specific Focused-Ion-Beam Lift-out Method for Cryo Transmission Electron Microscopy. J Struct Biol 2012, 180, 572-6.CrossRefGoogle ScholarPubMed
Schaffer, M.; Schaffer, B.; Ramasse, Q., Sample Preparation for Atomic-Resolution Stem at Low Voltages by Fib. Ultramicroscopy 2012, 114, 62-71.CrossRefGoogle ScholarPubMed
Sugar, J. D.; El Gabaly, F.; Chueh, W. C.; Fenton, K. R.; Tyliszczak, T.; Kotula, P. G.; Bartelt, N. C., High-Resolution Chemical Analysis on Cycled Lifepo4 Battery Electrodes Using Energy-Filtered Transmission Electron Microscopy. Journal of Power Sources 2014, 246, 512-521.CrossRefGoogle Scholar
Long, D.; McClary, S.; Hahn, N.; Zavadil, K.; Jungjohann, K., Chemistry, Microstructure, and Interphases of Magnesium Metal Anodes Captured Via Cryogenic Electron Microscopy. ECS Meeting Abstracts 2020, MA2020-02, 776-776.Google Scholar
Forero-Saboya, J.; Davoisne, C.; Dedryvère, R.; Yousef, I.; Canepa, P.; Ponrouch, A., Understanding the Nature of the Passivation Layer Enabling Reversible Calcium Plating. Energy & Environmental Science 2020.CrossRefGoogle Scholar