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Synthesis and Characterization of Cassava Bark Nanoparticles

Published online by Cambridge University Press:  30 April 2018

F.O. Kolawole ,
S.K. Kolawole ,
J.O. Agunsoye ,
S.A. Bello ,
J.A. Adebisi ,
W.O. Soboyejo  and
S.B. Hassan
F.O. Kolawole*
Affiliation:
Department of Materials and Metallurgical Engineering, Federal University, Oye-Ekiti, Nigeria Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria
S.K. Kolawole
Affiliation:
National Agency for Science and Engineering Infrastructure, Abuja, Nigeria
J.O. Agunsoye
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria
S.A. Bello
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria Department of Materials Science and Engineering, Kwara State University, Malete, Nigeria
J.A. Adebisi
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria Department of Metallurgical and Materials Engineering, University of Ilorin, IlorinNigeria
W.O. Soboyejo
Affiliation:
Department of Mechanical and Aerospace Engineering, Princeton University, New Jersey, U.S.
S.B. Hassan
Affiliation:
Department of Metallurgical and Materials Engineering, University of Lagos, Lagos, Nigeria
*
*Corresponding Author: funsho.kolawole@fuoye.edu.ng or fkopresido@yahoo.com
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Abstract

Synthesis and characterization of cassava bark nanoparticles (CBNPs) was carried out using ball milling at 36, 48, 60 and 72 hours. The morphology study was done using SEM and the Gwyddion software was used to determine the particle sizes from the SEM images. The particle distribution for the un-milled cassava bark (CB) was between 1.25 + 0.06 to 19.92 + 1.00 µm, while after milling for 36, 48, 60 and 72 hours the average particle size were 4.07 + 0.20, 4.00 + 0.20 µm, 80.90 + 4.05, 74.50 + 3.73 nm respectively. 13.68 + 0.68 nm was obtained by XRD using Scherrer equation after milling for 72 hours and the XRD results revealed the presence of compounds such as SiO2, CaCO3 and KAlSi3O8. TEM was used to determine nanoparticle size distribution after milling for 72 hours and the particle size ranged from 9.73 + 0.49 to 114.60 + 5.73 nm for cassava bark nanoparticles (CBNPs), EDX results showed trace element of Si, Ca, K, Fe, Al, O in the CB milled for 72hours.

Keywords

nanostructuresynthetic
Type
Articles
Information
MRS Advances , Volume 3 , Issue 42-43: African Materials Research Society 2017 , 2018 , pp. 2519 - 2526
Copyright
Copyright © Materials Research Society 2018 

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