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Epitaxy of Nb3 Sn Films on Sapphire

Published online by Cambridge University Press:  26 February 2011

A. F. Marshall
Affiliation:
Center for Materials Research, Stanford University, Stanford, CA 94305
F. Hellman
Affiliation:
Center for Materials Research, Stanford University, Stanford, CA 94305
B. Oh
Affiliation:
Center for Materials Research, Stanford University, Stanford, CA 94305
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Abstract

Films of Nb3Sn vapor deposited at low rates and high temperatures on (1102) sapphire form an epitaxial <100> single crystal matrix with a domain structure of misoriented regions bounded by low-angle dislocation boundaries. Nucleation of other orientations at the interface result in a highly oriented but polycrystalline film through approximately the first thousand Angstroms of film thickness. After this point random orientations become overgrown by epitaxial <100> regions. At slightly lower temperatures many small <100> grains with a second epitaxial relationship also nucleate at the interface. These rotated grains persist through greater thicknesses than random orientations. The misorientation defect structure of the single crystal matrix is analyzed by transmission electron microscopy.

Type
Research Article
Copyright
Copyright © Materials Research Society 1985

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References

1) Talvacchio, J., Ph. D. Thesis, Stanford University (1982).Google Scholar
2) Jacobson, B. E., Hammond, R. H., Geballe, T. H., and Salem, J. R., J. Less Common Metals 62 (1978) 59.Google Scholar
3) Hamar-Thibault, S. and Trilhe, J., J. Electrochem. Soc.: Solid State Science & Tech., 128 (1981) 581.Google Scholar
4) Kitano, Y., Nissen, H-U., Schauer, W., and Yin, D., Proc. of 17th Intl. Conf. on Low Temp. Phys. (1984) 615.Google Scholar
5) Hellman, F., Rudman, D. A., Hammond, R. H. and Geballe, T. H., Bull. Am. Phys. Soc. 28 (1983) 262.Google Scholar
6) Hellman, F. and Geballe, T. H., Bull. Am. Phys. Soc. 29 (1984) 385.Google Scholar