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Mechanical and Electrical Properties of Electroplated Copper Thin Films Used for Thin Film Interconnection

Published online by Cambridge University Press:  01 February 2011

Murata Naokazu
Affiliation:
naokazu.murata@rift.mech.tohoku.ac.jp, Fracture and Reliability Research Institute, Graduate School of Engineering, Tohoku University, sendai, Japan
Kinji Tamakawa
Affiliation:
kinji.tamakawa@rift.mech.tohoku.ac.jp, Fracture and Reliability Research Institute, Graduate School of Engineering, Tohoku University, sendai, Miyagi, Japan
Ken Suzuki
Affiliation:
kn@rift.mech.tohoku.ac.jp, Fracture and Reliability Research Institute, Graduate School of Engineering, Tohoku University, sendai, Miyagi, Japan
Hideo Miura
Affiliation:
hmiura@rift.mech.tohoku.ac.jp, Fracture and Reliability Research Institute, Graduate School of Engineering, Tohoku University, Sendai, Miyagi, Japan
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Abstract

Micro-texture dependence of both the mechanical and electrical properties of electroplated copper thin films was discussed experimentally considering the change of their micro texture caused by thermal history after the electroplating. Both the static and fatigue strength of the films changed drastically depending on the micro texture and it was found that there were two fatigue fracture modes in the films. One was a typical ductile intragranular fracture and the other was brittle intergranular one. The reason for the variation of the strength of the electroplated copper thin films was attributed to the variation of the average grain size and the characteristics of grain boundaries. In addition, the electrical reliability of the electroplated copper interconnections was discussed under electromigration tests. Though abrupt fracture mode due to the local fusion appeared in the as-electroplated films, the life of the interconnections was improved significantly after the annealing at temperatures high than 200°C. Typical change of the surface morphology of the film, i.e., the formation of voids and hillocks were observed on their surfaces after the annealing. This was also caused by the change of the micro texture from fine grains with porous grain boundaries to coarsened columnar grains with rigid grain boundaries. However, the stress-induced migration appeared in the annealed narrow interconnections, in particular. This was because of high tensile residual stress occurred in the film due to the constraint of the shrinkage of the films by rigid oxide around them. These results clearly indicated that the control of both the micro-texture and residual stress is indispensable for improving the reliability of the interconnectins.

Type
Research Article
Copyright
Copyright © Materials Research Society 2010

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References

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