Hostname: page-component-77c89778f8-gq7q9 Total loading time: 0 Render date: 2024-07-17T12:35:53.402Z Has data issue: false hasContentIssue false

Nanoindentation Induced Fracture in Hard Multilayer Thin Films

Published online by Cambridge University Press:  21 March 2011

A. Karimi
Affiliation:
Department of Physics, Swiss Federal Institute of Technology (EPFL) CH – 1015 Lausanne, Switzerland
D. Bethmont
Affiliation:
Department of Physics, Swiss Federal Institute of Technology (EPFL) CH – 1015 Lausanne, Switzerland
Y. Wang
Affiliation:
Department of Physics, Swiss Federal Institute of Technology (EPFL) CH – 1015 Lausanne, Switzerland
Get access

Abstract

Depth sensing nanoindentation and nanoscratch testing were combined with atomic force microscopy (AFM) and electron microscopy observations to study mechanical properties and fracture behavior of a number of TixAl1-xNyC1-y hard thin films. Various failure modes were activated either by normal loading-unloading or by microscratching of the samples to provide an estimation of the fracture toughness and interfacial fracture energies. By changing chemical composition and deposition conditions various nanostructured thin films including monolitically grown single layer, nanocomposite, and multilayers were coated onto the tungsten carbide-cobalt substrates. All tested films exhibit elevated mechanical properties with high hardness (38 – 45 GPa) and modulus (500 – 570 GPa). Under sufficiently high load indentation the formation of corner Palmqvist type radial cracks were usually observed because of small modulus mismatch between coating and substrate, good adhesion, and in particular high toughness of both substrate and films in spite of great difference in their respective hardness. Various failure modes were activated and the sequences of fracture events were determined using stepwise or continuously increasing load scratch tests. Some other films were found to be more sensitive to tensile stress behind the indenter which generates regularly repeated microcracks on the scratch track. Other films in particular multilayers were appeared more susceptible to compressive stress ahead of the indenter leading to local delamination at the interface between layers and the formation of irregular microcracks under the contact zone.

Type
Research Article
Copyright
Copyright © Materials Research Society 2002

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Prengel, H.G., Jindal, P.C., Wendt, K.H., Santhanam, A.T., Pedge, P.L., Penich, R.M., Surf. Coat. Technol 139 25 (2001).Google Scholar
2. Harris, S.G., Vlasveld, A.C., Doyle, E.D., Dolder, P.j., Surf. Coat. Technol 133–134 383 (2000).Google Scholar
3. Musil, J., Hruby, H., Thin Solid Films 365, 104 (2000).Google Scholar
4. , Levi, Kaplan, W.D., Bamberger, M., Materials Letters 35, 344 (1998).Google Scholar
5. Donohue, L.A., Smith, I.J., Münz, W.D. et al. Surf. Coat. Technol 94–95, 226 (1997).Google Scholar
6. Andersen, K.N., Bienk, E.J. et al. Surf. Coat. Technol 123, 219 (2000).Google Scholar
7. Prengel, H.G., Santhanam, A.T. et al Surf. Coat. Technol 94–95, 597 (1997).Google Scholar
8. Clements, B.M., Kung, H., Barnett, S.A., MRS Bulletin 24(2), 20 (1999).Google Scholar
9. Giannakopoulos, A.E., Thin Solid Films 372, 172(1998).Google Scholar
10. Tsui, T.Y., Vlassak, J., Nix, D., J. Mater. Res.14, part I 2196 and part II 2204 (1999).Google Scholar
11. Kriese, M.D., Moody, N.R., Gerberich, W.W., Acta Metall. Mater. 46, 6623(1998).Google Scholar
12. Hovsepian, P.E., Lewis, D.B., Münz, W.D., Surf. Coat. Technol 94–95, 226 (1997).Google Scholar
13. Bhattacharya, A.K., Nix, W.D., Int. J. Solids Structures 24 (12), 128 (1988).Google Scholar
14. Tuck, J.R., Korsunsky, A.M., Bhat, D.G., Bull, S.J., Surf. Coat. Technol 139, 63(2001).Google Scholar