Hostname: page-component-7479d7b7d-t6hkb Total loading time: 0 Render date: 2024-07-11T07:26:02.891Z Has data issue: false hasContentIssue false

Probing Water Dynamics in Octahedral Molecular Sieves: High Speed 1H MAS NMR Investigations

Published online by Cambridge University Press:  26 February 2011

Todd M. Alam
Affiliation:
tmalam@sandia.gov, Sandia National Laboratories, Nanostructured and Electronic Materials, 1515 Eubank SE,, MS 0886, Albuquerque, NM, NM, 87185-0886, United States, (505) 844-1225
Jason Pless
Affiliation:
djpless@sandia.gov, Sandia National Laboratories, Modelling and Simulation, Albuquerque, NM, 87185, United States
Tina M. Nenoff
Affiliation:
tmnenof@sandia.gov, Sandia National Laboratories, Surface and Interface Sciences, Albuquerque, NM, 87185-1415, United States
Get access

Abstract

The water dynamics in molecular sieve materials are probe using high speed proton magic angle spinning NMR spectrscopy

Type
Research Article
Copyright
Copyright © Materials Research Society 2007

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

[1]. Nyman, M.; Tripathi, A.; Parise, J. B.; Maxwell, R. S.; Harrison, W. T. A.; Nenoff, T. M., J. Am. Chem. Soc. 123, 1529 (2001).Google Scholar
[2]. Nyman, M.; Tripathi, A.; Parise, J. B.; Maxwell, R. S.; Nenoff, T. M., J. Am. Chem. Soc. 124, 1704 (2002).Google Scholar
[3]. Goldfarb, D.; Li, H.-X.; Davis, M. E., J. Am. Chem. Soc. 114, 3690 (1992).Google Scholar
[4]. Duer, M.; He, H.; Kolodziejski, W.; Klinowski, J., J. Phys. Chem. 98, 1198 (1994).Google Scholar
[5]. Benedetto, S. Di; Chidichimo, G.; Golemme, A.; Imbardelli, D., J. Phys. Chem. 100, 8079 (1996).Google Scholar
[6]. Chidichimo, G.; Golemme, A.; Imbardelli, D.; Santoro, E., J. Phys. Chem. 94, 6826 (1990).Google Scholar
[7]. Stepanov, A. G.; Shegai, T. O.; Luzgin, M. V.; Essayem, N.; Jobic, H., J. Phys. Chem. 107, 12438 (2003).Google Scholar
[8]. Mizuno, M.; Hamada, Y.; Kitahara, T.; Suhara, M., J. Phys. Chem. A 103, 4981 (1999).Google Scholar
[9]. Wingen, A.; Basler, W.; Lechert, H., Anisotropic Motion of Water in Zeolites EMT, L, and ZSM-5 as Studied by D- and H-NMR Line Splitting. In Progress in Zeolite and Microporous Materials, Chon, H.; Ihm, S.-K.; Uh, Y.S., Eds. Elsevier Science B. V.: 1997; Vol.105, pp 495.Google Scholar
[10]. Kobe, J. M.; Gluszak, T. J.; Dumesic, J. A.; Root, T. W., J. Phys. Chem. 99, 5485 (1995).Google Scholar
[11]. Bielecki, A.; Burum, D. P., Journal of Magnetic Resonance, Series A 116, 215 (1995).Google Scholar
[12]. Takahashi, T.; Kawashima, H.; Sugisawa, H.; Baba, T., Solid State Nuclear Magnetic Resonance 15, 119 (1999).Google Scholar
[13]. Schnell, I.; Spiess, H. W., J. Mag. Res. 151, 153 (2001).Google Scholar
[14]. Holland, G. P.; Cherry, B. R.; Alam, T. M., J. Magn. Reson. 167, 161 (2004).Google Scholar
[15]. Alam, T. M.; Nyman, M.; Cherry, B. R.; Segall, J. M.; Lybarger, L. E., J. Am. Chem. Soc. 126, 5610 (2004).Google Scholar
[16]. Abragam, A., Principles of Nuclear Magnetism. Clarendon Press: Oxford, 1961; p 599.Google Scholar
[17]. Batamack, P.; Dorémieux-Morin, C.; Vincent, R.; Fraissard, J., Chem. Phys. Lett. 180, 545 (1991).Google Scholar
[18]. Batamack, P.; Dorémieux-Morin, C.; Vincent, R.; Fraissard, J., J. Phys. Chem. 97, 9779 (1993).Google Scholar
[19]. Udea, T.; Nakamura, N., J. Phys. Chem. B 107, 13681 (2003).Google Scholar
[20]. Tritt-Goc, J.; Pislewski, N., Molecular Physics 83, 949 (1994).Google Scholar