Hostname: page-component-5c6d5d7d68-sv6ng Total loading time: 0 Render date: 2024-08-23T06:26:25.486Z Has data issue: false hasContentIssue false
  • English
  • Français

Viscoelastic Characterization of Polymers Using Dynamic Instrumented Indentation

Published online by Cambridge University Press:  01 February 2011

C. C. White ,
P. L. Drzal  and
M. R. VanLandingham
C. C. White*
Affiliation:
National Institute of Standards and Technology Gaithersburg, MD 20899–8615
P. L. Drzal
Affiliation:
National Institute of Standards and Technology Gaithersburg, MD 20899–8615
M. R. VanLandingham
Affiliation:
Weapons & Materials Research Directorate, ATTN: AMSRD-ARL-WM-MA, Army Research Laboratory, Aberdeen Proving Ground, Maryland.
*
1 Address all correspondence to this author; email: christopher.white@nist.gov
Get access

Abstract

Dynamic nanoindentation was performed on a poly(methyl methacrylate, PMMA), and two different poly(dimethyl siloxane, PDMS) samples having different crosslink densities. Comparison was made between dynamic nanoindentation and rheological instrumentation measurements in the glassy and rubbery plateau regions of polymeric materials. Excellent agreement between bulk rheological data and dynamic nanoindentation data was observed for the two glassy materials and the less compliant of the two PDMS samples. Results were divergent for the more compliant PDMS sample.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 841: Symposium R – Fundamentals of Nanoindentation and Nanotribology III , 2004 , R5.3
Copyright
Copyright © Materials Research Society 2005

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Oliver, W.C.; Pharr, G. M. J. Mater. Res. 1992, 7, 1564.Google Scholar
2. Lucas, B.N.; Oliver, W. C.; Swindeman, J. E. Materials Research Society, Boston, MA., 1998, pp 3–14.Google Scholar
3. White, C.C.; Drzal, P. L.; VanLandingham, M. R. Journal of Polymer Science, Polymer Physics in review.Google Scholar
4. Ferry, J. D. Viscoelastic Properties of Polymers; John Wiley & Sons, Inc: New York, 1980.Google Scholar
5. Asif, S.A.S.; Wahl, K. J.; Colton, R. J. Rev. Sci. Instrum. 1999, 70, 2408–2413.Google Scholar
6. Lu, H.; Wang, B.; Huang, G.; Viswanathan, H. Mechanics of Time-Dependent Materials 2003, 7, 189–207.Google Scholar
7. Oliver, W.C.; Pharr, G. M. J. Mat. Research 2004, 19, 3–20.Google Scholar
8. Pethica, J.B.; Oliver, W. C. Physica Scripta 1987, T19, 61–66.Google Scholar
9. Johnson, K.L.; Kendall, K.; Roberts, A. D. Proc. R. Soc. Lond. A 1971, 324, 301–313.Google Scholar