Hostname: page-component-78c5997874-94fs2 Total loading time: 0 Render date: 2024-11-18T05:51:47.129Z Has data issue: false hasContentIssue false

Improved Dispersion of Silicon Nitride Whiskers

Published online by Cambridge University Press:  15 February 2011

Wei-Heng Shih
Affiliation:
Department of Materials Engineering, Drexel University, Philadelphia, PA 19104
Michael Buchta
Affiliation:
Department of Materials Engineering, Drexel University, Philadelphia, PA 19104
Get access

Abstract

To improve the dispersion of silicon nitride whiskers in aqueous suspensions, a standard dispersant used in glass fiber industry, 3-aminopropyltriethoxysilane (APS) is added. It was found that the viscosity of the whisker suspensions is lowered and the centrifuged density of the suspensions is increased with the addition of the APS. The pH values of suspensions before and after the addition of APS indicate that APS extracts H+ ions from the solutions and the adsorption of APS on silicon nitride is saturated in our experiment. Our results indicate a colloidal route to the processing of ceramic composites with silicon nitride whiskers as reinforcements.

Type
Research Article
Copyright
Copyright © Materials Research Society 1995

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Hirata, Y., Nakagama, S., and Ishihara, Y., J. Mater. Res., 5 (3), 640646 (1990).Google Scholar
2. Vivilecchia, R., Cotter, R., Limpert, R., Thimot, N., and Little, J., J. Chromatography, 99, 407–24 (1974).Google Scholar
3. Waddell, T. G., Leyden, D. E., and DeBello, M. T., J. Am. Chem. Soc., 103, 5303–7 (1981).Google Scholar
4. Shih, W.-H., Pwu, L.-L., and Tseng, A. A., J. Am. Ceram. Soc., in press, (1995).Google Scholar