Hostname: page-component-78c5997874-xbtfd Total loading time: 0 Render date: 2024-11-19T09:26:25.156Z Has data issue: false hasContentIssue false

Mass Spectrometry Analysis of Organic-Inorganic Nanomaterials and their Precursors

Published online by Cambridge University Press:  01 February 2011

Jean-Jacques Gaumet
Affiliation:
LSMCL, Metz University, IPEM, Technopôle 2000, 57078 Metz Cedex 03, FRANCE
Geoffrey Strouse
Affiliation:
UCSB, Department of Chemistry, Santa Barbara, CA 93106-9510, U.S.A.
Get access

Abstract

We report in this paper how electrospray mass spectrometry (ESMS) and nanospray mass spectrometry (NMS) are promising for analyzing precursors and nano-scale semiconductor (IIVI) materials up to 1.5 nm and mixed valence clusters (Co/Cd). We show that both ion modes in ESMS and NMS provide insight concerning the structure analysis, the composition and the stability of these materials.

Type
Research Article
Copyright
Copyright © Materials Research Society 2002

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Shen, Y. Friend, C.S. Jiang, Y. Jakubczyk, D. Swiatkiewicz, J. Prasad, P.N. J. Phys. Chem. B 104, 1577 (2000).Google Scholar
2. Alivisatos, A. P. Science 271, 933 (1996).Google Scholar
3. Nanoscale Materials Special Issue, edited by Barbara, P.F. and Heath, J.R. (Acc. Chem. Res. 32, 1999) pp. 387454.Google Scholar
4. Farneth, W. E. Herron, N. Wang, Y. Chem. Mater. 4, 916 (1992).Google Scholar
5. Curri, M. L. Agostiano, A. Manna, L. Monica, M. D. Catalano, M. hiavarone, L. Spagnolo, V. Lugara, M. J. Phys. Chem. B, 104 (35), 8391 (2000).Google Scholar
6. Cumberland, S. L. Strouse, G. F. Mat. Res. Soc. Symp. Proc., 642, J7.8 (2001).Google Scholar
7. Herron, N. Calabrese, J. C. Farneth, W. E. Wang, Y. Science, 259, 1426 (1993).Google Scholar
8. Dance, I.G. Choy, A. Scudder, M. L. J. Am. Chem. Soc., 106, 6285 (1984).Google Scholar
9. Lee, G. S. H. Craig, D. C. Ma, I. Scudder, M. L. Bailey, T. D. Dance, I. G. J. Am. Chem. Soc., 110, 4863 (1988).Google Scholar
10. Gaumet, J. J. Strouse, G. F. J. Am. Soc. Mass Spectrom. 11, 338 (2000).Google Scholar
11. Gaumet, J. J. Khitrov, G. A. Strouse, G. F. Nano Lett., (2002) (in press).Google Scholar