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Powder diffraction data for the new aliphatic-aromatic thiodiols

Published online by Cambridge University Press:  06 March 2012

S. Pikus ,
E. Olszewska ,
W. Podkościelny ,
M. Rogulska  and
A. Kultys
S. Pikus*
Affiliation:
Department of Crystallography, Faculty of Chemistry, Maria Curie Sklodowska University, Pl. Marii Curie-Sklodowskiej 3, 20-031 Lublin, Poland
E. Olszewska
Affiliation:
Department of Crystallography, Faculty of Chemistry, Maria Curie Sklodowska University, Pl. Marii Curie-Sklodowskiej 3, 20-031 Lublin, Poland
W. Podkościelny
Affiliation:
Department of Organic Chemistry and Technology, Faculty of Chemistry, Maria Curie Sklodowska University, ul. Gliniana 33, 20-614 Lublin, Poland
M. Rogulska
Affiliation:
Department of Organic Chemistry and Technology, Faculty of Chemistry, Maria Curie Sklodowska University, ul. Gliniana 33, 20-614 Lublin, Poland
A. Kultys
Affiliation:
Department of Organic Chemistry and Technology, Faculty of Chemistry, Maria Curie Sklodowska University, ul. Gliniana 33, 20-614 Lublin, Poland
*
a)Electronic mail: stanpik@hermes.umcs.lublin.pl
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Abstract

Five new aliphatic-aromatic thiodiols: 1,2-bis[4-(2′-hydroxyethylthio)phenyl]ethane (C18H22O2S2), 1,2-bis[4-(3′-hydroxypropylthio)phenyl]ethane (C20H26O2S2), 1,2-bis[4-(6′-hydroxyhexylthio)phenyl]ethane (C26H38O2S2), 1,2-bis[4-(10′-hydroxydecylthio)phenyl]ethane (C34H54O2S2), 1,2-bis[4-(11′-hydroxyundecylthio)phenyl]ethane (C36H58O2S2) have been characterized by X-ray powder diffraction. These thiodiols can be used for synthesis of thermoplastic nonsegmented polyurethanes. Experimental 2θ peaks positions, relative peak intensities, values of d and Miller indices as well as unit cell parameters are reported.

Type
New Diffraction Data
Information
Powder Diffraction , Volume 18 , Issue 3 , September 2003 , pp. 240 - 243
Copyright
Copyright © Cambridge University Press 2005

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