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X-ray powder diffraction data for 17-hydroxy-16-methyl-9,11-epoxypregna-1,4,6-triene-3,20-dione, C22H26O4

Published online by Cambridge University Press:  16 July 2019

Q. Wang Open the ORCID record for Q. Wang [Opens in a new window] ,
X. Bian  and
X. Chen
Q. Wang*
Affiliation:
School of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China
X. Bian
Affiliation:
School of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China
X. Chen
Affiliation:
School of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China
*
a)Author to whom correspondence should be addressed. Electronic mail: qingwang@yzu.edu.cn; jstxwangqing@163.com.
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Abstract

X-ray powder diffraction data, unit-cell parameters, and space group for 17- hydroxy-16-methyl-9,11-epoxypregna-1,4,6-triene-3,20-dione, C22H26O4, are reported [ a = 18.435(1) Å, b = 12.269(3) Å, c = 8.251(5) Å, α = 90°, β = 90°, γ = 90°, unit-cell volume V = 1866.43 Å3, Z = 4, ρcal = 1.261 g cm−3 and space group P212121]. All measured lines were indexed and are consistent with the P212121 space group. No detectable impurities were observed.

Keywords

pharmaceutical intermediateanticoagulantdexamethasone
Type
Data Report
Information
Powder Diffraction , Volume 34 , Issue 3 , September 2019 , pp. 279 - 281
Copyright
Copyright © International Centre for Diffraction Data 2019 

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References

Boultif, A. and Louër, D. (1991). “Indexing of powder diffraction patterns for low-symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987–993.Google Scholar
Formica, F. A., Barreto, G., and Zenobi-Wong, M. (2019). “Cartilage-targeting dexamethasone prodrugs increase the efcacy of dexamethasone,” J. Control. Release 295, 118–129.Google Scholar
Hossain, M. S., Rashid, M., Babu, A. R., Saha, D., and Banik, D. (2018). “Betamethasone gel versus intravenous dexamethasone as prophylaxis against postoperative sore throat,” Delta Med. Col. J. 6(2), 73–77.Google Scholar
Lin, X., Wang, Q., Peng, X. L., and Li, H. (2017). “The binding properties of metandienone and human serum albumin by comparing with other five similar compounds,” J. Biochem. Mol. Toxicol. 31, e21866.Google Scholar
Pawley, G. S. (1981). “Unit-cell refinement from powder diffraction scans,” J. Appl. Crystallogr. 14(6), 357–361.Google Scholar
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