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Feasibility of X-ray fluorescence imaging in a SEM using pinhole relay optics

Published online by Cambridge University Press:  15 May 2001

D. Erre*
Affiliation:
Dynamique des Transferts aux Interfaces (DTI) (CNRS UMR 6107), Faculté des Sciences, BP 1039, 51687 Reims Cedex 2, France
H. Jibaoui
Affiliation:
Dynamique des Transferts aux Interfaces (DTI) (CNRS UMR 6107), Faculté des Sciences, BP 1039, 51687 Reims Cedex 2, France
S. Rondot
Affiliation:
Dynamique des Transferts aux Interfaces (DTI) (CNRS UMR 6107), Faculté des Sciences, BP 1039, 51687 Reims Cedex 2, France
D. Mouze
Affiliation:
Dynamique des Transferts aux Interfaces (DTI) (CNRS UMR 6107), Faculté des Sciences, BP 1039, 51687 Reims Cedex 2, France
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Abstract

The feasibility of imaging by X-ray fluorescence in a SEM has been tested on a simple laboratory set-up. It has been demonstrated that images generated by the fluorescent X-rays can be directly obtained with the use of simple pinhole relay optics and an incident X-ray beam created in a SEM. These images were acquired with a charge coupled device (CCD) camera coupled to a phosphor screen by a fibre-optic faceplate. This technique provides chemical and topographical images with a spatial resolution in the object plane of a few micrometres. This “global” imaging has the advantage that the acquisition time is only a few minutes for a sample surface of a few mm2.

Keywords

Type
Research Article
Copyright
© EDP Sciences, 2001

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References

Morton, R.W., Witherspoon, K.C., Adv. X-Ray Anal. 36, 97 (1992).
Iida, A., Noma, T., Adv. X-Ray Anal. 38, 283 (1995).
Dozier, C., Newman, D., Gilfrich, J., Freitag, R., Adv. X-Ray Anal. 37, 499 (1994).
Vincze, L., Janssens, K., Adams, F., Adv. X-Ray Anal. 37, 553 (1994).
Van Langevelde, F., Bowen, D., Tros, G., Vis, R., Huizing, A., De Boer, D., Nucl. Instrum. Methods A 292, 719 (1990). CrossRef
Iida, A., Noma, T., Nucl. Instrum. Methods B 82, 129 (1993). CrossRef
Gurker, N., Adv. X-Ray Anal. 23, 263 (1979).
Gurker, N., Adv. X-Ray Anal. 30, 53 (1986).
Martin, A.P., Brunton, A.M., Fraser, G.W., Holland, A.D., Keay, A., Hill, J., Nelms, N., Turcu, I.C.E., Allott, R., Lisi, N., Spencer, N., X-Ray Spectrom. 28, 64 (1999). 3.0.CO;2-T>CrossRef
Erre, D., Thomas, X., Mouze, D., Patat, J.M., Trebbia, P., Cazaux, J., Surf. Interface Anal. 19, 89 (1992). CrossRef
Erre, D., Bourelle, E., Claude-Montigny, B., Métrot, A., Cazaux, J., Phys. Rev. B 56, 4944 (1997). CrossRef
H. Jibaoui, Microscopie X par réflexion totale et par fluorescence, Ph.D. thesis, University of Reims, 1999.
J.M. Wulveryck, Contribution à la mise au point d'une microscopie X quantitative avec une source X polychromatique, Ph.D. thesis, University of Reims, 1999.
Ross, P.A., J. Opt. Soc. Am. 16, 433 (1928). CrossRef
Kirkpatrick, P.K., Rev. Sci. Instrum. 15, 223 (1944). CrossRef
Dothie, J.J., Galle, B., Spectrochim. Acta 20, 1735 (1964). CrossRef
Cazaux, J., X-Ray Spectrom. 28, 9 (1999). 3.0.CO;2-L>CrossRef
Hiraga, J., Tsunemi, H., Yoshita, K., Miyata, E., Ohtani, M., Jap. J. Appl. Phys. 37, 4627 (1998). CrossRef
K. Sakurai, Spectrochim. Acta 54, Part B, 1497 (1999).