The emergence and widespread distribution of eye fibulae as adornment objects, from the northern provinces of the Roman Empire to northeastern Europe and Scandinavia, as well as their typology have been widely explored. Currently in Lithuania, a total of 209 eye fibulae dating to the 1st and 2nd centuries are known. The geographical distribution, typology and chronology of these Early Roman Period jewelry artifacts do not present any problem. However, the technology of manufacture of these fibulae has been much less studied. The present article analyzes the technology of manufacture of Prussian series eye fibulae, including the previously unknown specific manufacturing techniques, such as the use of wooden axes to modify the construction of the fibula and make it more durable and long lasting. Radiocarbon (14C) dating has unambiguously confirmed that the wooden axes are contemporaneous with the time of the use of the fibulae, while observation under the scanning electron microscope has identified wood species used for making the wooden axes. The X-ray fluorescence spectrometry (XRF) analysis was used to determine the copper alloys, of which eye fibulae were made. The manufacturing technologies of eye fibulae (forging and casting) are discussed in the context of analytical and experimental studies.

Here we report radiocarbon measurements made on wheat seed tissue (Triticum aestivum L.; winter or spring type growth habit), from the seed archive of the IPK Gatersleben, Sachsen-Anhalt, Germany, which was harvested between 1946 and 2020. The results give an overview of 75 years of radiocarbon concentration evolution in agricultural plant products. The wheat tissue radiocarbon concentrations follow known pre- and post-bomb radiocarbon records, such as the atmospheric Jungfraujoch, Schauinsland, and NH1 datasets. Based on a Northern Hemisphere growing period from April to July, the Gatersleben seed tissue radiocarbon concentration indicates incorporation of fossil carbon of about 1% with respect to the high alpine, clean-air CO2 of the Jungfraujoch station between 1987 and 2019. We propose to use the pre- and post-bomb radiocarbon record of Gatersleben wheat as a reference in forensic investigations, such as the age estimation of paper by analyzing starch used in paper manufacture. Additionally, an advantage of the record reported here lies in its extensibility by adding new analyses from future harvests.

The function and change of global soil carbon (C) reserves in natural ecosystems are key regulators of future carbon-climate coupling. Microbes play a critical role in soil carbon cycling and yet there is poor understanding of their roles and C metabolism flexibility in many ecosystems. We wanted to determine whether vegetation type and climate zone influence soil microbial community composition (fungi and bacteria) and carbon resource preference. We used a biomarker (phospholipid fatty acids, PLFAs), natural abundance 13C and 14C probing approach to measure soil microbial composition and C resource use, along a 1900–4167-m elevation gradient on Mount Gongga (7556 m asl), China. Mount Gongga has a vertical mean annual temperature gradient of 1.2–10.1°C and a diversity of typical vegetation zones in the Tibetan Plateau. Soils were sampled at 10 locations along the gradient capturing distinct vegetation types and climate zones from lowland subtropical-forest to alpine-meadow. PLFA results showed that microbial communities were composed of 2.1–51.7% bacteria and 2.0–23.2% fungi across the elevation gradient. Microbial biomass was higher and the ratio of soil fungi to bacteria (F/B) was lower in forest soils compared to meadow soils. δ13C varied between −33‰ to −17‰ with C3 plant carbon sources dominant across the gradient. Soil organic carbon (SOC) turnover did not vary among three soils we measured from three forest types (i.e., evergreen broadleaved subtropical, mixed temperate, coniferous alpine) and dissolved organic carbon (DOC) turnover decreased with soil elevation. Forest soil microbial PLFA 14C and δ13C measurements showed that forest type and climate were related to different microbial C use. The 14C values of microbial PLFAs i15, a15, 16:1, br17 decreased with elevation while those of C16:0, cyC17, and cyC19 did not show much difference among three forest ecosystems. Bacteria and bacillus represented by C16:1 and brC17 showed considerable microbial C metabolism flexibility and tended to use ancient carbon at higher altitudes. Anaerobes represented by cyC17 and cyC19 showed stronger C metabolism selectivity. Our findings reveal specific C source differences between and within soil microbial groups along elevation gradients.

Archaeological excavations unearthed three burial mounds between 1983 and 1986 at Fehérvárcsurgó (Hungary). Based on the archaeological determination the site was dated to the Early Iron Age. A complex wooden architecture was observed in the largest tumulus containing inner and outer beam constructions separated by stone blocks. Dendrochronological and radiocarbon (14C) analyses were performed on conserved logs (n=5) to constrain the felling date of the timber, identified as oak, and the construction period of the tumuli. The four longest ringwidth series were synchronized providing a 153-yr-long floating chronology. Five blocks were removed from the cross sections and accelerator mass spectrometry (AMS) 14C analysis was performed on the separated α-cellulose. A wiggle-matching procedure was employed as the 14C ages were in agreement with their relative position in the tree-ring sequence and concurred with the expected archaeological period. The calibrated age range of the last extant ring is 747–707 cal BC (95.4%). The earliest possible felling date of the trees used in the construction was between 735 and 695 BC considering the missing sapwood. This is the first 14C dated tree-ring width chronology from the Early Iron Age in Hungary providing a valuable reference for dendroarchaeological studies along the eastern border of the Hallstatt Culture.

The Suyanggae archeological complex is located in Aegok-li, Danyang County, Chungbuk Province, Korea (128°20'00"E, 365˚7'15"N, elevation 132 m). We investigated two Suyanggae Paleolithic localities (1 and 6). A total of 31 samples (18 localities) were analyzed for radiocarbon (14C) ages in three paleolithic cultural horizons of Suyanggae Locality 6 (SYG-6). The purpose of this paper is to report all dating results of SYG-6. It was found that ranges of 14C ages (BP) of cultural layers of SYG-6 are known to be 17,550 ± 80 ∼ 20,470 ± 70, 30,360 ± 350 ∼ 44,100 ± 1900, and 34,870 ± 540 ∼ 46,360 ± 510 BP for cultural layers 2, 3, and 4, respectively. We compared these age data with those of the previous study associated with Gunang Cave near Suyanggae Locality 1 (SYG-1). Based on the chronological information of the three archaeological sites, early humans lived in a rather cold environment from approximately 30,000 to 46,000 BP and disappeared between 30,000 ∼ 20,000 BP and then settled again in SYG-6 site during LGM period. This study demonstrates that archaeological study is important not only for understanding human occupations with their cultural development but also establishing climatic signals to which they have been adapted as a part of the human evolutional process.

A laboratory intercomparison project was carried out on 20 annually resolved late-wood samples from the Danish oak record. The project included the following three laboratories: (1) the University of Arizona AMS Laboratory, University of Arizona, USA (AA); (2) HEKAL AMS Laboratory, MTA Atomki, Hungary (DeA); and (3) Aarhus AMS Centre (AARAMS), Aarhus University, Denmark (AAR). The large majority of individual data points (96%) lie within ±2σ of the weighted mean. Further assessment of the accuracy associated with the individual laboratories showed good agreement, indicating that consistent and reliable 14C measurements well in agreement with each other are produced at the three laboratories. However, the quoted analytical uncertainties appear to be underestimated when compared to the observed variance of differences from the geometric mean of the samples. This study provides a general quality check of the single-year tree-ring 14C measurements that are included in the new calibration curve.

Tel Hazor is one of only a few sites in Israel where remains of the Intermediate Bronze Age (IBA) in the second half of the 3rd millennium BC were found on top of Early Bronze III (EB III) city remains. A probe excavation was held at Hazor in 2017 to explore the chronological relation between the EB III and the IBA occupation. The radiocarbon (14C) absolute dates generated from this probe excavation show that following the EB III city demise, the site was abandoned for up to a few hundred years before it was resettled in the IBA. 14C dates obtained from the last level of the EB III city are well before 2500 BCE, fully aligned with the recent “High Chronology” for the EBA in the southern Levant. The excavation also produced dates associated with IBA “Black Wheel-Made Ware” vessels, which were found in large numbers at Hazor.

Archaeologists have been using luminescence to date pottery in South America since the late 1970s, inspired by early success in northern Chile. However, luminescence dates have not been rigorously compared to independent dating methods, which this paper’s goal. First, we present a compilation of 94 paired 14C and luminescence dates from the southern Andes, which reveals discrepancies across a range of contexts and ages. Second, we compare two Bayesian models of sets of 14C and thermoluminescence (TL) dates from three ceramic styles in the Azapa Valley, Chile, and the Inca occupation of Mendoza, Argentina. We find that only the 14C models produce results that agree with expectations based on independent data. Third, we present results from a pilot study in Mendoza that dated 6 sherds with 3 luminescence methods each and closely associated 14C dates. The reasons for disagreement between methods remain unclear, but Andean sediments with low and unstable luminescence sensitivity seem to be an important factor. Even though some luminescence ages are accurate, the clear trend of inconsistent results leads us to recommend that archaeologists use 14C rather than luminescence dates to build cultural chronologies.

The paper explores the emergence and development of arable farming in southeastern Norway by compiling and analyzing directly dated cereals from archaeological contexts. By using summed probability distributions of radiocarbon dates and Bayesian modeling, the paper presents the first comprehensive analysis of the directly dated evidence for farming in the region. The models provide a more precise temporal resolution to the development than hitherto presented. The results demonstrate that the introduction of arable farming to southeastern Norway was a long-term development including several steps. Three different stages are pointed out as important in the process of establishing arable farming: the Early and Middle Neolithic, the Late Neolithic, and the Early Iron Age.

The Early and Middle Bronze Age in the Carpathian Basin is often viewed as a long period of transition from a dispersed form of land occupation to one of increasing aggregation, ultimately resulting in the formation of tell settlements and large cemeteries. This developmental trajectory remains a legacy of early 20th century archaeology, where the similarity of material culture recovered from cemeteries and settlements was used to develop a multi-linear scheme of progression of regional chronologies tied to specific archaeological cultures. While typologically conclusive, the recent increase in the availability of radiocarbon determinations suggests that these sequences represent a priori interpretation of social development rather than empirically verified observations. In order to do so, it is necessary to re-evaluate the existing dataset in order to determine whether the formation of tells was a chronologically contemporary development and whether the regional chronological sequences are supported by independent dating.

In this paper we discuss recent developments in documenting the spread of millet across the Eurasian steppes. We emphasize that, despite a recent proposal that millet consumption in southern Siberia can be attributed to the Early Bronze Age (i.e., the late third to early second millennium BC), at present there are no direct data for southern Siberia indicating the consumption of millet prior to the Late Bronze Age, from the 14th century BC. We also present in full the combined stable isotope and 14C datasets from the Minusinsk Basin to support this conclusion.

Radiocarbon (14C) is an isotopic tracer used to address a wide range of scientific research questions. However, contamination by elevated levels of 14C is deleterious to natural-level laboratory workspaces and accelerator mass spectrometer facilities designed to precisely measure small amounts of 14C. The risk of contaminating materials and facilities intended for natural-level 14C with elevated-level 14C-labeled materials has dictated near complete separation of research groups practicing profoundly different measurements. Such separation can hinder transdisciplinary research initiatives, especially in remote and isolated field locations where both natural-level and elevated-level radiocarbon applications may be useful. This paper outlines the successful collaboration between researchers making natural-level 14C measurements and researchers using 14C-labeled materials during a subglacial drilling project in West Antarctica (SALSA 2018–2019). Our strict operating protocol allowed us to successfully carry out 14C labeling experiments within close quarters at our remote field camp without contaminating samples of sediment and water intended for natural level 14C measurements. Here we present our collaborative protocol for maintaining natural level 14C cleanliness as a framework for future transdisciplinary radiocarbon collaborations.

This paper presents results of accelerator mass spectrometry radiocarbon (AMS 14C) dating of prehistoric samples (human and animal bones, cremated human bones, charcoals, and other charred plant macroremains) from archaeological sites located in the area of Dobużek Scarp, on the Sokal Ridge in central-eastern Poland (E Poland). The date list reports 46 14C age measurements performed within the project “The Dobużek Scarp Microregion as a part of a physiological and biocultural frontier between the Baltic and the Pontic zone (from the 6th to the 2nd millennium BC)” conducted in 2016–2021. The resulting 14C dates fall into quite a long interval, which in terms of the regional archaeological periodization lasts from the Middle Eneolithic to the Early Iron Age, and in terms of the climatological one corresponds with the Subboreal.