Hostname: page-component-586b7cd67f-tf8b9 Total loading time: 0 Render date: 2024-11-23T14:07:52.242Z Has data issue: false hasContentIssue false

A Method for Obtaining a Quantitative Pole Figure of Stretched Rubber

Published online by Cambridge University Press:  06 March 2019

Otto Renius*
Affiliation:
Detroit Arsenal, Center Line, Michigan
Get access

Abstract

Work at the Detroit Arsenal has shown that techniques similar to those employed for the determination of pole figures of metals can be utilized for studying organic materials such a a stretched rubber latex. The rubber, when stretched, forms a preferred orientation pattern which is proportional in intensity to the degree of elongation, and which can be used to plot a pole figure.

A Geiger-counter spectrometer was used to study samples of rubber stretched 600 to 1000 per cent. Using a transmission technique, the specimens were tilted to the impinging X-ray beam in five degree increments while rotating through 360 degrees to allow the measurement of the diffracted beam from the selected atomic planes at various angles within the specimen. The intensities of the diffracted beam at these angles were plotted on a stereographic net to form the pole figures of the (002) and (012) planes of the stretched rubber. The geometry of the sample arrangements permitted the outer portion of the pole figure to be plotted from alpha angle 0 degrees to alpha angle 45 degrees.

Type
Research Article
Copyright
Copyright © International Centre for Diffraction Data 1957

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

1. Katz, J. R., Kolloid Z. 36, 300; 37, 19(1925).Google Scholar
2.National Bureau of Standards RP 1039 October 1937.Google Scholar
3. Lotmar, W. and Meyer, K. H., Monatsh. 69, 115(1936).Google Scholar
4.ASTM Standards, E 81-49 T (2) (1949).Google Scholar
5. Geisler, A. H., G. E. Research Report # RL-790, Jan. 1953.Google Scholar