Hostname: page-component-586b7cd67f-t7fkt Total loading time: 0 Render date: 2024-11-23T08:32:50.076Z Has data issue: false hasContentIssue false

Effect of initial preform porosity on solid-state foaming of titanium

Published online by Cambridge University Press:  01 May 2006

N.G.D. Murray
Affiliation:
Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208
D.C. Dunand*
Affiliation:
Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208
*
b) Address all correspondence to this author. e-mail: dunand@northwestern.edu
Get access

Abstract

Titanium foams were produced by the expansion of pressurized argon pores trapped within a preform during a previous powder-consolidation step. Compared with creep expansion at 903 °C, superplastic expansion (induced by a 830–980 °C cycling around the allotropic temperature of titanium) increases foaming rate and final porosity. The pore size and fraction in the preforms were varied by using a range of initial titanium powder sizes and argon pressures. As initial preform porosity increases from 0.06 to 2.7%, foaming rate increases in the early stages of creep and superplastic foaming. However, at a later stage, foaming ceases prematurely for preforms with high initial porosity, as pores connect to the surface, allowing the escape of the pressurized argon. Preforms with 0.40% initial porosity result in foams with an optimal combination of high foaming rate, high final porosity (up to 47%), tailorable open or closed porosity, and Young's modulus as low as 23 GPa.

Type
Articles
Copyright
Copyright © Materials Research Society 2006

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1.Dunand, D.C.: Processing of titanium foams. Adv. Eng. Mater. 6, 369 (2004).CrossRefGoogle Scholar
2.Kearns, M.W., Blenkinsop, P.A., Barber, A.C., Farthing, T.W.: Manufacture of a novel porous metal. Int. J. Powder Metall. 24, 59 (1988).Google Scholar
3.Queheillalt, D.T., Choi, B.W., Schwartz, D.S., Wadley, H.N.G.: Creep expansion of porous Ti-6Al-4V sandwich structures. Metall. Mater. Trans. A 31, 261 (2000).CrossRefGoogle Scholar
4.Queheillalt, D.T., Gable, K.A., Wadley, H.N.G.: Temperature dependent creep expansion of Ti-6Al-4V low density core sandwich structures. Scripta Mater. 44, 409 (2001).CrossRefGoogle Scholar
5.Elzey, D.M., Wadley, H.N.G.: The limits of solid state foaming. Acta Mater. 49, 849 (2001).CrossRefGoogle Scholar
6.Vancheeswaran, R., Queheillalt, D.T., Elzey, D.M., Wadley, H.N.G.: Simulation of the creep expansion of porous sandwich structures. Metall. Mater. Trans. A 32, 1813 (2001).CrossRefGoogle Scholar
7.Davis, N.G., Teisen, J., Schuh, C., Dunand, D.C.: Solid-state foaming of titanium by superplastic expansion of argon-filled pores. J. Mater. Res. 16, 1508 (2001).CrossRefGoogle Scholar
8.Murray, N.G.D., Dunand, D.C.: Microstructure evolution during solid-state foaming of titanium. Compos. Sci. Technol. 63, 2311 (2003).CrossRefGoogle Scholar
9.Murray, N.G.D., Schuh, C.A., Dunand, D.C.: Solid-state foaming of titanium by hydrogen-induced internal-stress plasticity. Scripta Mater. 49, 879 (2003).CrossRefGoogle Scholar
10.Murray, N.G.D., Dunand, D.C.: Effect of thermal history on the superplastic expansion of argon-filled pores in titanium: Part 1— Kinetics and microstructure. Acta Mater. 52, 2269 (2004).CrossRefGoogle Scholar
11.Murray, N.G.D., Dunand, D.C.: Effect of thermal history on the superplastic expansion of argon-filled pores in titanium: Part 2— Modeling of kinetics. Acta Mater. 52, 2279 (2004).CrossRefGoogle Scholar
12.Li, H.L., Oppenheimer, S.M., Stupp, S.I., Dunand, D.C., Brinson, L.C.: Effects of pore morphology and bone ingrowth on mechanical properties of microporous titanium as an orthopaedic implant material. Mater. Trans. 45, 1124 (2004).CrossRefGoogle Scholar
13.Ashby, M.F., Evans, A., Fleck, N.A., Gibson, L.J., Hutchinson, J.W., Wadley, H.N.G.: Metal Foams: A Design Guide (Butterworth-Heinemann, Boston 2000).Google Scholar
14.Greenwood, G.W., Johnson, R.H.: The deformation of metals under stress during phase transformations. Proc. R. Soc. London 283A, 403 (1965).Google Scholar
15.Zwigl, P., Dunand, D.C.: Transformation superplasticity of zirconium. Metall. Mater. Trans. A 29, 2571 (1998).CrossRefGoogle Scholar
16.Dunand, D.C., Bedell, C.M.: Transformation-mismatch superplasticity in reinforced and unreinforced titanium. Acta Mater. 44, 1063 (1996).CrossRefGoogle Scholar
17.Frost, H.J., Ashby, M.F.: Deformation-Mechanism Maps: The Plasticity and Creep of Metals and Ceramics (Pergamon Press, Oxford, 1982).Google Scholar
18.Reed, J.S.: Introduction to the Principles of Ceramic Processing (John Wiley, New York, 1988).Google Scholar
19.Eshelby, J.D.: The determination of the elastic field of an ellipsoidal inclusion, and related problems. Proc. R. Soc. London A241, 376 (1957).Google Scholar
20.Gibson, L.J., Ashby, M.F.: Cellular Solids (Cambridge University Press, 1997).CrossRefGoogle Scholar
21.Zhao, Y.H., Tandon, G.P., Weng, G.J.: Elastic-moduli for a class of porous materials. Acta Mech. 76, 105 (1989).CrossRefGoogle Scholar
22.Weng, G.J.: The theoretical connection between Mori Tanaka theory and the Hashin Shtrikman Walpole bounds. Int. J. Engng. Sci. 28, 1111 (1990).CrossRefGoogle Scholar
23.Wanner, A.: Elastic-modulus measurements of extremely porous ceramic materials by ultrasonic phase spectroscopy. Mater. Sci. Eng. A 248, 35 (1998).CrossRefGoogle Scholar
24.Rho, J.Y., Ashman, R.B., Turner, C.H.: Young's modulus of trabecular and cortical bone material—ultrasonic and microtensile measurements. J. Biomech. 26, 111 (1993).CrossRefGoogle ScholarPubMed
25.Ashman, R.B., Rho, J.Y.: Elastic-modulus of trabecular bone material. J. Biomech. 21, 177 (1988).CrossRefGoogle ScholarPubMed
26.Donachie, M.J.: Biomedical alloys. Adv. Mater. Proc. 7, 63 (1998).Google Scholar
27.Simske, S.J., Ayers, R.A., Bateman, T.A.: Porous materials for bone engineering. Mater. Sci. Forum 250, 151 (1997).CrossRefGoogle Scholar