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The study of ultrasound-assisted extraction of flavonoids from Polygonum cuspidatum Sieb. et Zucc.

Published online by Cambridge University Press:  29 April 2019

Weiwei Jia ,
Zhenbin Chen ,
Yingyu Zhao ,
Ke Li ,
Brandon Tichnell ,
Zhenghua Tang ,
Juan M. Ruso  and
Zhen Liu Open the ORCID record for Zhen Liu [Opens in a new window]
Weiwei Jia
Affiliation:
College of Materials Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, China; and State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China
Zhenbin Chen*
Affiliation:
College of Materials Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, China; and State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China
Yingyu Zhao
Affiliation:
College of Materials Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, China; and State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China
Ke Li*
Affiliation:
College of Materials Science and Engineering, Lanzhou University of Technology, Lanzhou 730050, China; and State Key Laboratory of Gansu Advanced Non-ferrous Metal Materials, Lanzhou University of Technology, Lanzhou 730050, China
Brandon Tichnell
Affiliation:
Department of Physics and Engineering, Frostburg State University, Frostburg, Maryland 21532, USA
Zhenghua Tang
Affiliation:
Guangzhou Key Laboratory for Surface Chemistry of Energy Materials, New Energy Research Institute, School of Environment and Energy, South China University of Technology, Guangzhou Higher Education Mega Centre, Guangzhou 5100067, China; and Guangdong Provincial Key Laboratory of Atmospheric Environment and Pollution Control, Guangdong Provincial Engineering and Technology Research Center for Environmental Risk Prevention and Emergency Disposal, School of Environment and Energy, South China University of Technology, Guangzhou Higher Education Mega Centre, Guangzhou 510006, China
Juan M. Ruso
Affiliation:
Soft Matter and Molecular Biophysics Group, Department of Applied Physics, University of Santiago de Compostela, Santiago de Compostela 15782, Spain
Zhen Liu*
Affiliation:
Department of Physics and Engineering, Frostburg State University, Frostburg, Maryland 21532, USA
*
a)Address all correspondence to these authors. e-mail: zhenbinchen@163.com
b)e-mail: zhenliu8@gmail.com
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Abstract

In this work, flavonoids in Polygonum cuspidatum Sieb. et Zucc. were extracted by ultrasound-assisted methodology and determined by ultraviolet–visible spectrophotometry. After that, extraction conditions were optimized by the single fact investigation, the central composite design, and response surface methodology (RSM) in turn. The results showed the optimal values of ethanol concentration, solid–liquid ratio, extraction temperature, extraction time, ultrasonic power, and number of extraction times were 60%, 1:20 (g/mL), 45 °C, 34 min; 80 W, and 5, respectively. The extraction ratio of flavonoids could be as high as 94.50%. The influence order of each factor was ultrasonic power > extraction time > extraction temperature > ethanol concentration. The results also showed that the experimental value was close to the predicted value (94.49%) of the established model by RSM, which proved that the established model was reasonable. The thermodynamic results showed that the extraction process was endothermic and could proceed spontaneously.

Keywords

biologicalchemical compositionethanol
Type
Invited Paper
Information
Journal of Materials Research , Volume 34 , Issue 19: Focus Issue: Thermodynamics of Complex Solids , 14 October 2019 , pp. 3254 - 3262
Copyright
Copyright © Materials Research Society 2019 

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