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Probability of detection of internal voids in structural ceramics using microfocus radiographya)

Published online by Cambridge University Press:  31 January 2011

George Y. Baaklini
Affiliation:
Cleveland State University, Cleveland, Ohio 44115
Don J. Roth
Affiliation:
National Aeronautics and Space Administration, Lewis Research Center, Cleveland, Ohio 44135
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Abstract

The reliability of microfocus x radiography for detecting internal voids in structural ceramic test specimens was statistically evaluated. The microfocus system was operated in the projection mode using low x-ray photon energies (<20 keV) and a 10 μm focal spot. The statistics were developed for implanted internal voids in green and sintered silicon carbide and silicon nitride test specimens. These statistics were compared with previously obtained statistics for implanted surface voids in similar specimens. Problems associated with void implantation and characterization are discussed. Statistical results are given as probability-of-detection curves at a 95% confidence level for voids ranging in size from 20–528 μm in diameter.

Type
Articles
Copyright
Copyright © Materials Research Society 1986

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References

REFERENCES

1Harper, J. E., in Ceramics for High-Performance Applications HI: Reliability (Plenum, New York, 1983), pp. 645664.Google Scholar
2Shulz, R B., in Ref. 1, pp. 2128.Google Scholar
3Evans, A. G., in Defect Properties and Processing of High Technology Nonmetallic Materials (North-Holland, New York, 1984), pp. 6380.Google Scholar
4Hall, W. B. and Nichols, R. L., in Research Reports: 1984 NASA/ASEE Summer Faculty Fellowship Program, NASA Report No. CR-171317, 1985.Google Scholar
5Mieskowski, D. M., Sanders, W. A., and Pierce, L. A., NASA Report No. TM-87092, 1985.Google Scholar
6Evans, A. G., Kino, G. S., Khuri-Yakub, B. T., and Tittman, B. R., Mater. Eval. 35 (4), 85 (1977).Google Scholar
7Teotia, A. P. S. and Johnson, L. R., Structural Ceramics in Transportation: Fuel Implications and Economic Impacts, CONF-850115-4, 1985.Google Scholar
8Klima, S. J., NASA Report No. TM-86949, 1984.Google Scholar
9Baaklini, G. Y., Kiser, J. D., and Roth, D. J., Adv. Ceram. Mater. 1 (1), 43 (1986); NASA Report No. TM-86945, 1984.Google Scholar
10Roth, D. J., Klima, S. J., Kiser, J. D., and Baaklini, G. Y., NASA Report No. TM-87035, 1985.Google Scholar
11Kupperman, D. S., Karplus, H. B., Poeppel, R. B., Ellingson, W. A., Burger, H., Robbins, C., and Fuller, E., Argonne National Laboratory Report No. ANL/FE-83–25, 1984.Google Scholar
12Roberts, R. A., Ellingson, W. A., and Vannier, M. W., in the Proceedings of the 15th Symposium on Nondestructive Evaluation, 1985 (to be published).Google Scholar
13Khandelwal, P. K., Kinnick, R. R., and Heitman, P. W., Am. Ceram. Soc. Bull. 64, 1112 (1985).Google Scholar
14Rice, R. W., Mecholsky, J. J., Frieman, S. W., and Morey, S. M., Naval Research Laboratory Report No. NRL-MR-4075, 1979 (AD-A078234).Google Scholar
15Nishida, K., “Silicon Nitride”, in The Development of Structural Fine Ceramics in Japan, The Japan Industrial and Technological Bulletin, (Japan External Trade Organization, Tokyo, 1983), pp. 2124.Google Scholar
16Rice, R. W., Freiman, S. W., Mecholsky, J. J. Jr., Ruh, R., and Harada, Y., in Ceramicsfor High Performance Applications II, edited by Burke, J. J., Lenoe, E. N., and Katz, R. N. (Brook Hill, Chestnut Hill, MA, 1977), pp. 669687.Google Scholar
17Rice, R. W., J. Mater. Sci. 19, 895 (1984).Google Scholar
18Halmshaw, R., Industrial Radiology (Applied Science, London, 1982).CrossRefGoogle Scholar
19McMaster, R., Nondestructive Testing Handbook (Ronald, New York, 1959), Vol. I, Chaps. 1327.Google Scholar
20Kooswsky, R., in Ceramicsfor High Performance Applications, edited by Burke, J. J., Gorum, A. E., and Katz, R. N. (Brook Hill, Chestnut Hill, MA, 1974), pp. 665685.Google Scholar
21Richerson, D. W. and Johansen, K. M., Garret Turbine Engine Co. Report No. REPT-21-4410, 1982 (AD-A117088).Google Scholar
22Parish, R. W., in Nondestructive Inspection Methods for Propulsion Systems and Components AGARD-LS-103 (Advisory Group for Aerospace Research and Development, Nevilly-Sur-Seine, France, 1979) (AD-AD69901).Google Scholar
23Smith, R. L. Jr., J. Non-Destr. Test 22, 236 (1980).Google Scholar
24Radiological Health Handbook (U. S. Department of Health, Education, and Welfare, Washington, DC, 1970), pp. 137140.Google Scholar
25Packman, P. F., Klima, S. J., Davies, R. L., Malpani, J., Moyzis, J., Walker, W., Yee, B. G. W., and Johanson, D. P., in Metals Handbook, edited by Boyer, H. E. (American Society for Metals, Metals Park, OH, 1976), 8th ed., Vol. 11, pp. 414424.Google Scholar
26Dutta, S., J. Mater. Sci. 19, 1307 (1984).CrossRefGoogle Scholar