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Surface nanodeformation of discontinuously reinforced Ti composite by in situ atomic force microscope observation

Published online by Cambridge University Press:  31 January 2011

Y. Tanaka*
Affiliation:
National Institute for Materials Science, Tsukuba, Ibaraki 305-0047, Japan
J.-M. Yang
Affiliation:
Department of Materials Science and Engineering, University of California, Los Angeles, California 90095-1595
Y.F. Liu
Affiliation:
Research Center for Advanced Science and Technology, The University of Tokyo, Meguro-ku, Tokyo 153-8505, Japan
Y. Kagawa
Affiliation:
National Institute of Materials Science, Tsukuba, Ibaraki 305-0047, Japan; and Research Center for Advanced Science and Technology, The University of Tokyo, Meguro-ku, Tokyo 153-8505, Japan
*
a)Address all correspondence to this author. e-mail: TANAKA.Yoshihisa@nims.go.jp
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Abstract

The surface nanodeformation of a discontinuously reinforced Ti–6Al–4V composite during tensile loading was investigated by in situ atomic force microscope (AFM) observation. The material used was a TiB whisker and TiC particle reinforced Ti–6Al–4V composite. The evolution of surface roughness and slip band spacing was quantified as a function of applied strain. The microstructural damage during tensile loading was also studied. The formation of slip bands within a grain of the Ti–6Al–4V matrix was clearly observed when the applied strain above was 1.3%. The amount of slip bands and surface roughness increase with increasing applied strain. The rupture of TiC particle and multiple cracking of TiB whiskers were also observed at the applied strain above 1.3%. The interaction of slip bands with the reinforcements and mechanisms of deformation and fracture of the composite were elucidated.

Type
Articles
Copyright
Copyright © Materials Research Society 2007

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References

REFERENCES

1Chandran, K.S. Ravi, Panda, K.B.Sahay, S.S.: TiBw-reinforced Ti composites: Processing, properties, application prospects, and research needs. JOM 56(5), 42 2004CrossRefGoogle Scholar
2Saito, T.: Automotive application of discontinuously reinforced TiB–Ti composites. JOM 56(5), 33 2004CrossRefGoogle Scholar
3Yolton, C.F.: The pre-alloyed powder metallurgy of titanium with boron and carbon additions. JOM 56(5), 56 2004Google Scholar
4Gorsse, S.Miracle, D.B.: Mechanical properties of Ti–6Al–4V/TiB composites with randomly oriented and aligned TiB reinforcements. Acta Mater. 51, 2427 2003CrossRefGoogle Scholar
5Soboyejo, W.O., Shen, W.Srivatsan, T.S.: An investigation of fatigue crack nucleation and growth in a Ti–6Al–4V/TiB in situ composite. Mech. Mater. 36, 141 2004CrossRefGoogle Scholar
6Ma, Z.Y., Tjong, S.C.Meng, X.M.: Creep behavior of in situ dual-scale particles—TiB whisker and TiC particulate-reinforced titanium composites. J. Mater. Res. 17, 2307 2002CrossRefGoogle Scholar
7Allais, L., Bornert, M., Bretheau, T.Caldemaison, D.: Experimental characterization of the local strain field in a heterogeneous elastoplastic material. Acta Metall. Mater. 42, 3865 1994Google Scholar
8Crostack, H.A., Fischer, G., Soppa, E., Schmauder, S.Liu, Y.L.: Localization of strain in metal matrix composites studied by scanning electron microscope-based grating method. J. Microsc. 201, 171 2001CrossRefGoogle ScholarPubMed
9Zheng, M.Y., Zhang, W.C., Wu, K.Yao, C.K.: The deformation and fracture behavior of SiCw/AZ91 magnesium matrix composite during in-situ TEM straining. J. Mater. Sci. 38, 2647 2003Google Scholar
10Buffiere, J.Y., Maire, E., Cloetens, P., Lormand, G.Fougeres, R.: Characterization of internal damage in a MMCp using x-ray synchrotron phase contrast microtomography. Acta Mater. 47, 1613 1999CrossRefGoogle Scholar
11Prangnell, P.B., Downes, T., Withers, P.J.Stobbs, W.M.: The deformation of discontinuously reinforced MMCs-I. The initial yielding behavior. Acta Metal. Mater. 42, 3437 1994CrossRefGoogle Scholar
12Llorca, J.Gonzalez, C.: Microstructural factors controlling the strength and ductility of particle-reinforced metal-matrix composites. J. Mech. Phys. Solids 46, 1 1998CrossRefGoogle Scholar
13Tong, W., Hector, L.G., Weiland, H.Wieserman, L.F.: In-situ surface characterization of a binary aluminum alloy during tensile deformation. Scripta Mater. 36, 1339 1997Google Scholar
14Harvey, S.E., Marsh, P.G.Gerberich, W.W.: Atomic force microscopy and modeling of fatigue crack initiation in metals. Acta Metall. Mater. 42, 3493 1994Google Scholar
15Gerberich, W.W., Harvey, S.E.Hoehn, J.W.: Low and high cycle fatigue—a continuum supported by AFM observations. Acta Mater. 46, 5007 1998CrossRefGoogle Scholar
16Cretegny, L.Saxena, A.: AFM characterization of the evolution of surface deformation during fatigue in polycrystalline copper. Acta Mater. 49, 3755 2001Google Scholar
17Ambard, A., Guetaz, L., Louchet, F.Guichard, D.: Role of interphases in the deformation mechanisms of an α/β titanium alloy at 20K. Mater. Sci. Eng., A 319–321, 404 2001Google Scholar
18Chandrasekaran, D.Nygards, M.: A study of the surface deformation behavior at grain boundaries in an ultra-low-carbon steel. Acta Mater. 51, 5373 2003CrossRefGoogle Scholar
19Tanaka, Y., Yang, J.M., Liu, Y.F.Kagawa, Y.: Characterization of nanoscale deformation in a discontinuously reinforced titanium composite using AFM and nanolithography. Scripta Mater. 56, 209 2007CrossRefGoogle Scholar
20Johnson, A.J.W., Bull, C.W., Kumar, K.S.Briant, C.L.: The influence of microstructure and strain rate on the compressive deformation behavior of Ti–6Al–4V. Metall. Mater. Trans. A 34, 295 2003Google Scholar
21Tvergaard, V.: Breakage and debonding of short brittle fibres among particulates in a metal matrix. Mater Sci. Eng., A 396, 192 2004Google Scholar
22Niordson, C.F.: Strain gradient plasticity effects in whisker-reinforced metals. J. Mech. Phys. Solids 51, 1863 2003Google Scholar
23Kim, Y-H., Lee, S.Kim, N.J.: Fracture mechanisms of a 2124 aluminum matrix composite reinforced with SiC whiskers. Metall. Trans. A23, 2589 1992CrossRefGoogle Scholar
24Khireddine, D., Rahouadj, R.Clavel, M.: Irreversibility of strain during low-cycle fatigue experiments of a precipitation-hardened alloy. Philos. Mag. A 77, 1555 1998Google Scholar
25Graf, M.Hornbogen, E.: The effect of inhomogeneity of cyclic strain on initiation of cracks. Scripta Metal. 12, 147 1978CrossRefGoogle Scholar
26Aveston, J.Kelly, A.: Theory of multiple fracture of fibrous composites. J. Mat. Sci. 8, 352 1973CrossRefGoogle Scholar
27Tvergaard, V.: Debonding of short fibres among particulates in a metal matrix composite. Int. J. Solids Structures 40, 6957 2003CrossRefGoogle Scholar