Hostname: page-component-5c6d5d7d68-wpx84 Total loading time: 0 Render date: 2024-08-27T09:21:05.943Z Has data issue: false hasContentIssue false

Nanoindentation Behavior of Gold Single Crystals

Published online by Cambridge University Press:  01 February 2011

Martha M. McCann
Affiliation:
Virginia Tech, Department of Materials Science and Engineering, Blacksburg, VA 24061
Sean G. Corcoran
Affiliation:
Virginia Tech, Department of Materials Science and Engineering, Blacksburg, VA 24061
Get access

Abstract

Nanoindentation is an increasingly used tool to investigate the mechanical properties of very small volumes of material. It is usually a very consistent measure of the elastic response of material and plastic response to point contact loading. Nanoindentation experiments on gold single crystals display tremendous variation in the residual deformation. The depth of penetration, which is vital in hardness determination, can differ by as much as 100%. This large variability of the load-depth data is usually explained by surface differences such as crystal orientation, oxide thic kness, presence of multiple solid phases, or contamination layers. None of these reasons apply to the variation observed in the gold system. The onset of plastic deformation is observed at a stress level on the order of the theoretical yield strength. The difference in depth of penetration is independent of this elastic -plastic transition. This paper reports on attempts to correlate the depth of penetration to surface feature size and surface preparation procedures.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Bahr, D.F., Watkins, C.M., Kramer, D.E., and Gerberich, W.W., MRS Proceedings, 522, 83, (1998).Google Scholar
2. Corcoran, S.G., Colton, R.J., Lilleodden, E.T., and Gerberich, W.W., Phys. Rev. B, 55 (24), R16057, (1997).Google Scholar
3. Kiely, J.D. and Houston, J.E., Phys.Rev. B, 57 (19), 12588, (1998).Google Scholar
4. Hay, J.L., O'Hern, M.E., and Oliver, W.C., MRS Proceedings, 522, 27 (1998).Google Scholar
5. Johnson, K.L., Kendall, K., and Roberts, A.D., Proc. R. Soc. Lond. A., 324, 301, (1971).Google Scholar
6. Latanision, R.M., Opperhauser, H. Jr, and Westwood, A.R.C., The Science of Hardness Testing and Its Research Applications, American Society for Metals, Ohio, (1973).Google Scholar
7. Pharr, G.M. and Oliver, W.C., J. Mat. Res., 4 (1), 94, (1989).Google Scholar
8. Fivel, M.C., Robertson, C.F., Canova, G.R., and Boulanger, L., Acta Mater, 46 (17), 6183, (1998).Google Scholar
9. Robertson, C.F. and Fivel, M.C., J. Mat. Res, 14 (6) 2251, (1991).Google Scholar
10. Grosskreutz, J.C., J. Electrochem. Soc., 116 (9), 1232, (1969).Google Scholar
11. Westwood, A.R.C., Preece, C.M., and Goldheim, D.L., Molecular Processes on Solid Surfaces, McGraw-Hill, New York, 591610, (1968).Google Scholar
12. Tambwe, M.F., Stone, D.S., Hirvonen, J.P., Suni, I., and Hannula, S.P., Scripta Mat., 37 (9), 1421, (1997).Google Scholar
13. Corcoran, S.G., Brankovic, S.R., Dimitrov, N., and Sieradzki, K., MRS Proceedings, 505, 77, (1998).Google Scholar
14. Bobij, M. S. and Biswas, S. K., J. Mat. Res., 13, 3227, (1998).Google Scholar
15. Streitz, F.H., Cammarata, R.C., and Sieradzki, K., Phys. Rev. B, 49 (15), 10 707, (1994)Google Scholar
16. Suresh, S., Nieh, T.-G., and Choi, B.W., Scripta Mater., 41 (9), 951, (1999).Google Scholar
17. Gouldstone, A., Koh, H.-J., Zeng, K.-Y., Giannakopoulos, A.E., and Suresh, S., Acta Mater., 48, 2277, (2000).Google Scholar
18. Bahr, D.F., Nelson, J.C., Tymiak, N.I., and Gerberich, W.W., J. Mat. Res., 12 (12), 3345, (1997).Google Scholar
19. Monocrystals, Inc. Cleveland, OHGoogle Scholar
20. Kiely, J.D., Hwang, R.Q., and Houston, J.E., Phys. Rev. Lett., 81 (20), 4424, (1998).Google Scholar
21. Hull, D. and Bacon, D.J., Introduction to Dislocations, Butterworth Hein Google Scholar