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Silver Nanoparticles for SERS Identification of Dyes

Published online by Cambridge University Press:  16 August 2012

Edgar Casanova-González ,
Angélica García-Bucio ,
José Luis Ruvalcaba-Sil ,
Víctor Santos-Vasquez ,
Baldomero Esquivel ,
María Lorena Roldán  and
Concepción Domingo
Edgar Casanova-González
Affiliation:
Departamento de Física Experimental, Instituto de Física, Universidad Nacional Autónoma de México, Circuito de la Investigación Científica s/n, Ciudad Universitaria, Mexico DF 04510, Mexico. e-mail: sil@fisica.unam.mx
Angélica García-Bucio
Affiliation:
Departamento de Física Experimental, Instituto de Física, Universidad Nacional Autónoma de México, Circuito de la Investigación Científica s/n, Ciudad Universitaria, Mexico DF 04510, Mexico. e-mail: sil@fisica.unam.mx
José Luis Ruvalcaba-Sil
Affiliation:
Departamento de Física Experimental, Instituto de Física, Universidad Nacional Autónoma de México, Circuito de la Investigación Científica s/n, Ciudad Universitaria, Mexico DF 04510, Mexico. e-mail: sil@fisica.unam.mx
Víctor Santos-Vasquez
Affiliation:
Coordinación Nacional de Conservación del Patrimonio Cultural, INAH, Mexico.
Baldomero Esquivel
Affiliation:
Instituto de Química, Universidad Nacional Autónoma de México, Mexico.
María Lorena Roldán
Affiliation:
Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006-Madrid, Spain.
Concepción Domingo
Affiliation:
Instituto de Estructura de la Materia, CSIC, Serrano 121, 28006-Madrid, Spain.
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Abstract

Coinage metals nanoparticles have been widely used in last decade for enhancing the Raman signal of a variety of compounds. Several preparation methods have been proposed, including chemical reduction of gold or silver salts with sodium citrate, hydroxylamine or sodium borohydride, microwave-assisted reduction with glucose, Tollens mirror, electrodeposition, vacuum evaporation and pulsed-laser deposition.

In this work, gold and silver nanoparticles were prepared by chemical reduction with sodium citrate and hydroxilmanine, characterized by UV-Vis spectroscopy and High Resolution Transmission Electronic Microscopy and tested as SERS substrate. Carminic acid, cochineal, axiote, muitle and zacatlaxcalli SERS spectra were recorded at different pH. Natural dyes samples were prepared by extraction from its natural sources, following traditional recipes. Although differs for each dye, best results were achieved by performing SERS experiments at pH neutral to basic.

Keywords

nanoscaleRaman spectroscopydye
Type
Articles
Information
MRS Online Proceedings Library (OPL) , Volume 1374: Symposium S8 – Cultural Heritage and Archaeological Issues in Materials Science , 2012 , pp. 263 - 274
Copyright
Copyright © Materials Research Society 2012

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