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Synthesis and Characterization of Novel Organic-Inorganic Nancomposite Coatings

Published online by Cambridge University Press:  01 February 2011

Brian P. Mosher
Affiliation:
North Carolina State University, Dept of Mechanical and Aerospace Engineering, Raleigh, NC 27695
Taofang Zeng
Affiliation:
North Carolina State University, Dept of Mechanical and Aerospace Engineering, Raleigh, NC 27695
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Abstract

In this paper, we report the synthesis and characterization of three novel water-based nanocomposite coatings. Throughout the paper, these coatings will be referred to as coatings 1, 2 and 3. The coatings are silica-based and are sol-gel derived using surfactant assemblies, with aluminum perchlorate as a catalyst. After synthesis, curing causes cross-link polymerization of silica, forming Si-O-Si network. The formation of this 3-Dimensional network can be verified using Fourier Transform Infrared Spectroscopy (FTIR) and Transmission Electron Microscopy (TEM). Incorporating metal oxide nanoparticles gives the material unique properties.

Type
Research Article
Copyright
Copyright © Materials Research Society 2004

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References

REFERENCES

1 Hench, L. L.; West, J K. Chem Rev 1990, 90, 33.Google Scholar
2 Brinker, C. J.; Scherer, G. W. Sol-Gel Science; The Physics and Chemistry of Sol-Gel Processing; Academic: New York, 1990.Google Scholar
3 Jang, K.; Park, H. Hyperstructured Organic Materials Research Center, School of Chemical Engineering, Seoul National University, San 56–1, Shinlimdong, Kwanakgu, Seoul 151742, KoreaGoogle Scholar
4 Seelinger, A.; Weiss, P. M.; Nguyen, A.; Lu, Y.; Assink, R. A.; Gong, W.; Brinker, C. J. Nature 1998, 294, 256.Google Scholar
5 Cassagneau, T.; Caruso, F. Oligosilsesquioxanes as Versatile Building Blocks for the Preparation of Self-Assemble Thin Films. JACS Articles, 2001.Google Scholar
6 Stein, A.; Melde, B. J.; Schroden, R. C. Adv. Mater. 1999, 11, 579.Google Scholar
7 Wei, Y.; Jin, D.; Brennan, D. J.; Rivera, D. N.; Zhuang, Q.; DiNardo, N. J.; Qiu, K. Chem. Mater. 1998, 10, 769772.Google Scholar
8 Grace DavisonGoogle Scholar
9 Bertduzza, A.; Fagnano, C.; Morelli, M.A.; Gotardi, V.; Guglielmi, M. J Non-Cryst Solids 1982, 48, 117.Google Scholar
10 Matos, M. C.; Ilharco, L. M.; Almeida, R. M. J Non-Cryst Solids 1992, 147–148, 232.Google Scholar
11 Li, Haoying, Chen, Yunfa: “Preparation of organic-inorganic multifunctional nanocomposite coating via sol-gel routes” from Journal of Nanoparticle Research 3: 159, 2001.Google Scholar