Hostname: page-component-586b7cd67f-vdxz6 Total loading time: 0 Render date: 2024-11-24T15:15:17.728Z Has data issue: false hasContentIssue false
  • English
  • Français

Trace Analysis of Nanoscale Materials by Analytical Electron Microscopy

Published online by Cambridge University Press:  21 February 2011

Dale E. Newbury  and
Richard D. Leapman
Dale E. Newbury
Affiliation:
National Institute of Standards and Technology, Gaithersburg, MD 20899
Richard D. Leapman
Affiliation:
National Institutes of Health, Bethesda, MD 20892
Get access

Abstract

Trace analysis of nanometer-scale objects can be performed with parallel-detection electron energy loss spectrometry in the analytical electron microscope. Spectra are collected in the second difference mode with the beam current chosen to maximize the spectral count rate. Numerous elements can be detected at trace levels below 100 parts per million atomic, including transition metal, alkali metal, alkaline earth, and rare earth elements, provided they have a “white line” resonance structure at the ionization edge. Trace nanoanalysis by AEM/PEELS permits direct examination of the microscopic distribution of trace constituents.

Type
Research Article
Information
MRS Online Proceedings Library (OPL) , Volume 332: Symposium U – Determining Nanoscale Physical Properties of Materials by Microscopy and Spectroscopy , 1994 , 287
Copyright
Copyright © Materials Research Society 1994

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

References

REFERENCES

1. Joy, D. C., Romig, A. D., and Goldstein, J. I., Principles of Analytical Electron Microscopy, (Plenum Press, New York, 1986).Google Scholar
2. Wittry, D. B., Proc. 9th Intl. Conf. X-ray Optics and Microanalysis, 14 (1980).Google Scholar
3. Leapman, R. D. and Newbury, D. E., Analytical Chem., 65, 2409 (1993).Google Scholar
4. Egerton, R. F., Electron Energy-Loss Spectroscopy in the Electron Microscope (Plenum Press, New York, 1986) 205.Google Scholar
5. Shuman, H. and Kruit, P., Rev. Sci. Instrum., 56, 231, (1985).Google Scholar